GCMS surrogate recovery results, sample AE07115, April 15, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File : C:\MSDCHEM\l\DATA\041002\7115.D Vial: 22 Acq On : 11 Apr 2002 7:15 am Operator: Bohlk Sample : SAMPLE 7115 3/27/02 Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 20 Octadecane, 1-chloro- Concentration Rank 19

R.T. EstConc Area Relative to ISTD R.T.

38.94 2.80 ug/L 258983 Perylene-dl2 34.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Octadecane, 1-chloro- 288 C18H37C1 003386-33-2 64 2 Nonahexacontanoic acid, propyl e... 1041 C72H144O2 040710-41-6 64 3 Tritetracontane 605 C43H88 007098-21-7 64 4 Heneicosane (CAS) $$ n-Heneicosane 296 C21H44 000629-94-7 64 Abundance Scan 6104 (38.944 min): 7115.D (-) m/z57.10100.00% 57

5000

■p

>141 38.60 38.80 39.00 39.20 04- 1111^14...^. ....... ........... m/z 71.10 52.61% m/z-> 0 100 200 300 400 500 600 700 800 900 1000 <Kbundance . #236018; Octadecane, 1-chloro- 57

5000 38.60 38.80 39.00 39.20 m/z 85.10 45.49%

I 11147 288 0^ m/z-> 0 100 200 300 400 500 600 700 800 900 1000 Abundance #391598; Nonahexacontanoic acid, propyl ester SS Propyl no... 57

38.60 38.80 39.00 39.20 5000 m/z 43.10 43.99% 1040

1 ,1?... ....... . , I.... 771.... 0t U ++ Tl/Z-> 0 100 200 300 400 500 600 700 800 900 EsE Abundance #382449: Tritetracontane 57 ■p 38.60 38.80 39.00 39.20 m/z 55.10 36.99%

5000

11 llW,,.225..309 393 491 575______________ 04- I ','r yr r.-1 (-t 1 1-111. i • ■ ■ ■ । ■ ■ ■ ■ । • ■ • ■ । ■ ■ ■ ■ । ■ m/z-> 0 100 200 300 400 500 600 700 800 900 iBHM 38.60 38.80 39.00 39.20

7115.D 5080402BB.M Mon Apr 15 18:16:44 2002 Page 23

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