GCMS pesticide analysis results, sample AE11573, May-June 2002

NYC 9/11 Public Portal Document Library Search Compound Report 0 Data File : C:\MSDCHEM\1\DATA\052902\11311RR.D Vial: 16 • Acq On : 29 May 2002 2:39 pm Operator: Bohlk / Inst 213 Sample : SAMPLE 11311 RE-EXTD 5/23/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1\5973N\052802.M (RTE Integrator) Title : Quantitation For Method 525.2 Library : C:\DATABASE\WILEY7N.L Peak Number 4 Tridecane (CAS) $$ n-Tridec... Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 15.57 0.08 ug/L 113059 Acenaphthene-diO 18.19 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tridecane (CAS) $$ n-Tridecane $— 184 C13H28 000629-50-5 72 2 Pentadecane (CAS) $$ n-Pentadecane 212 C15H32 000629-62-9 64 3 Hexadecane 226 C16H34 000544-76-3 59 4 Nonane, 5-butyl- $$ 5-Butylnonan... 184 C13H28 017312-63-9 59 Abundance Scan 495 (15.566 mln): 11311RR.D (-) m/z 71.10 100.00% 57 71 85 5000

99 113 9- 127 155169 AASANN m/z-> 01 —..... hal, 20 40 60 - 80 100 120 140 160 180 200 220 m/z 57.10 79.40%

Abundance #93376: Tridecane (CAS) $$ n-Tridecane $3 Tridecane, n- 43 517

5000 71 AANLALA 15.20 15.40 15.60 15.80 29 85 m/z 85.10 62.38%

01 ‘ I* IL‘1 • lpb _ 99 112 127 141 155 184 । .11 *ITatraa"s 1"i 1 fri TTr i i । ti i ! j i »■ i i) i i mfe-> 20 40I 60 80 100 120 140 160 180 200 220 Abundance #134014: Pentadecane (CAS) $$ n-Pentadecane

5000 43 57

71 AANUUA 15.20 15.40 15.60 15.80 m/z70.1027.77% 85 29 99 .. 01 — 4 ■ ■ A . 113 127 141.155 ..... 212 miz-> Abundance 20 40 60 80 100 120 140 160 180 200 220 57 #154904: Hexadecane AAAMANN 15*20 15*40 15.60 15*80 ’ ~ 43 m/z 55.10 25.47% 71 5000 85

29 99

m/z-> 0 -P 41,.1312711155169,183197,..228 20 40 60 80 100 120 140 160 180 200 220 15.20 15.40 15.60 15.80

.1311RR.D 052802.M Mon Jun 03 15:50:18 2002 Page 6

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