GCMS sample AE07115 results, April 25, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File : C:\MSDCHEM\l\DATA\041002\7115.D Vial: 22 Acq On : 11 Apr 2002 7:15 am Operator: Bohik Sample : SAMPLE 7115 3/27/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 19 Tridecane, 2-methyl- $$ 2-M... Concentration Rank 18

R.T. EstConc Area Relative to ISTD R.T.

37.72 5.58 ug/L 515015 Perylene-dl2 34.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tridecane, 2-methyl- $$ 2-Methyl... 198 C14H30 001560-96-9 64 2 Tetradecane, 6,9-dimethyl- 226 C16H34 055045-13-1 64 3 1-Iodoundecane $$ Undecane, 1-iodo- 282 C11H23I 004282-44-4 64 4 Pentadecane (CAS) $$ n-Pentadeca... 212 C15H32 000629-62-9 59 Abundance Scan 5896 (37.722 mln): 7115.D (-) m/z 57.10 100.00%

_N_ 57

85 5000

4 T 1* T T 37.40 37.60 37.80 38.00 1 i 1 113 140 mmAHn —mmmmmmp 183 m/z 85.10 54.36% 0 __ /z-> 0 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #113308: Tridecane, 2-methyl- $$ 2-Methyltridecane $$ 2-Me... 57

5000 41 85 37.40 37.60 37.80 38.00 m/z 71.10 47.81% 155 113 I 183 2 0 . ..... i■■ ■■i ■■•■ i ■ ■■■ i •n/z-> 0 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #154934: Tetradecane, 6,9-dimethyl- 57

37*40 37.60 37*80 38.00‘T 5000 m/z 43.10 43.22% 41 __ 85 155

m/z-> 0^ mH. .1113 .139 1 180 197 । f fi । T] । TTr UTT’ i <i 11 r 111 > ii # । > 0 20 40 60 80 100 120 140 160 180 200 220 240 260 280 226

Abundance #227492: 1-lodoundecane $$ Undecane, 1-lodo- 57 1111 ‘1' I ‘1111111 rI+7’1 > ( 37.40 37.60 37.80 38.00 m/z 55.10 23.42%

5000 4'1

113 85

11129 155 AA m/z—> 0—T N5-M4 I 183 211 i । 282 > 11 j 11 H j > > > > । > > • 11 (> 11 j 11 • 11 >) < 11 > > > 11 f > 0 20 40 60 80 100 120 140 160 180 200 220 240 260 280 37.40 37.60 37*80 38.00 T

7115. D 5080402BBC.M Tue Apr 23 15:53:10 2002 Page 22

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