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GCMS sample AE07110 results, April 25, 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry analysis results for sample AE07110 including detection of unknown compounds.

NYC-WTC_000049027–000049062

Folder label: “GCMS X 4/12/02 A 4/23/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\ 041002\7110.D Vial: 17 Acq On : 11 Apr 2002 3:12 am Operator: Bohik Sample : SAMPLE 7110 3/27/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 19 Hexatriacontane Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

35.78 4.81 ug/L 440668 Perylene-dl2 34.01

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 91 2 Tetradecane (CAS) $$ n-Tetradeca... 198 C14H30 000629-59-4 87 3 Pentatriacontane 493 C35H72 000630-07-9 86 4 Heptadecane $$ n-Heptadecane $$ ... 240 C17H36 000629-78-7 86 Abundance Scan 5565 (35.777 mln): 7110.D (-) m/z 57.10 100.00% 57

5000 85 • 1 I t I ‘ 4 35.40 35.60 35.80 36.00 0- Immmmmmmmmnmmmmmmmmmpu | 113, 141 . 207 m/z 71.10 57.98% m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #369892: Hexatriacontane 57

5000 85 35.40 35.60 35.80 36.00 TT‘ 41 m/z 43.15 39.80%

m/z-> Abundance

5000 0 113,141 . 169 197 225 TTMTTPmmmmmpp 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 #113293: Tetradecane (CAS) $$ n-Tetradecane $$ Isotetradecane 57 "wMMow TI T LT 35.40 35.60 35.80 36.00 m/z 85.15 T 38.62% Tit

41 85 A m/z—> Abundance 0 4.4 113 4 141 169 THTmTmmTTTT 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 57 #367079: Pentatriacontane *MMWwyya ‘I T T T v "W*w ■R 35.40 35.60 35.80 36.00 m/z 55.10 24.85%

/z—> 5000

0 4'1

umnayr 85

113 1e,,6.11A/192, 197,725,253 „ 281,39% 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 MyMwty* k "Wwp ■ i ■ ‘11 i • ■ • ‘ i ■ • ■ ■ i ■ ‘ 35.40 35.60 35.80 36.00 ■ i •

7110.D 5080402BBC.M Tue Apr 23 15:52:29 2002 Page 21

NYC-WTC_000049060

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NYC-WTC_000049060Source: NYC Law Department, mirrored locally

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