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GCMS sample AE07115 results, April 25, 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry analysis results for sample AE07115 including detection of unknown compounds.

NYC-WTC_000049063–000049101

Folder label: “GCMS X 4/12/02 A 4/23/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data Pile : C:\MSDCHEM\l\DATA\041002\7115.D Vial: 22 Acq On : 11 Apr 2002 7:15 am Operator: Bohik Sample : SAMPLE 7115 3/27/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BB.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 18 Hexatriacontane Concentration Rank 16

R.T. EstConc Area Relative to ISTD R.T.

36.68 14.90 ug/L 1376280 Perylene-d12 34.02

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Hexatriacontane 507 C36H74 000630-06-8 91 2 Heneicosane (CAS) $$ n-Heneicosane 296 C21H44 000629-94-7 91 3 Hexatriacontane $$ n-Hexatriacon... 507 C36H74 000630-06-8 90 4 Dotriacontane_________________________ 451 C32H66 000544-85-4 90 Abundance Scan 5719 (36.682 min): 7115.D (-) m/z 57.10 100.00% 57

5000 85

36.40 36.60 36.80 37.00 .. ....................................................... m/z 71.10 68.60% 0- miz-> 0 50 100 150 200 250 300 350 400 450 500 Abundance #369892: Hexatriacontane 57

5000 ‘I T T TUB 85 36.40 36.60 36.80 37.00 m/z 43.15 47.61% __ _ . I 113141169197225_________________ 0- ah"f 44 fs* * »*| i »■» Fri 111 j > । । > j < । > • । > > "rpr i 111 11 miz-> 0 50 100 150 200 250 300 350 400 450 500 Abundance #245747: Heneicosane (CAS) $$ n-Heneicosane 57 36.40 36.60 36.80 37.00 5000 m/z 85.10 43.12% 85

113141169197 239 296 0- ■ W ----------------- m/z-> 0 50 100 150 200 250 300 350 400 450 500 Abundance #369895: Hexatriacontane $$ n-Hexatriacontane 57 T T T T 36.40 36.60 36.80 37.00 m/z 55.10 25.39% ... 5000 85

29 113 0- 1 1,4 169197225253281309337 379 421449477506 4*50448100 m/z—> 0 150 200 250 300 350 400 450 500 36.40 36.60 36.80 37.00

7115.D 5080402BBC.M Tue Apr 23 15:53:09 2002 Page 21

NYC-WTC_000049098

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NYC-WTC_000049098Source: NYC Law Department, mirrored locally

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