GCMS sample results AE11284, DEP Labs, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\020516\11284.D Vial: 12 Acq On : 16 May 2002 8:14 pm Operator: Nefliu Sample : sample Inst : Instrumen . Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 6 Decane Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 11.12 2.03 ug/1 116349 1,4-Dichlorobenzene-d4 11.37 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Decane 142 C10H22 000124-18-5 87 2 1-Octanol, 2-butyl- 186 C12H260 003913-02-8 83 3 Decane 142 C10H22 000124-18-5 83 4 Nonane 128 C9H20 000111-84-2 78 Abundance Scan 1369 (11.123 min): 11284D (-1359) (-) m/z 57.10 100.00% 43 57

X 5000 71 85 r ehre pe ।

miz-> Abundance - u 4— l 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 #109556: Decane 99 112 -PP .. ।;.., ।.... (. । /... 1.... ।,... ।.. 142 m/z 10.80 11.00 11.20 11.40 43.05 83.55%

43 57

5000 wW/A T"I 71 10.80 11.00 11,20 11.40 29 85 m/z 41.10 41.92%

n/z-> 15 " i ■ ■" i ■ ■ mH I 99 113 142 tr . . [ il q l . . I'l i . . > | l'. . I | . . . , | . i . . | I . . , j II II I i i II | 1 i 10 20 30 40 50 S) 70 80 90 100 110 120 130 140 150 160 170 Abundance #112292:1-Octanol, 2-butyl- 43 57

10.80 11.00 11.20 11.40 5000 71 m/z 71.20 28.81% 29 85 I 9 111 125 140 154 168 n/z-> + L | i i n n i , HH reTmmpmmmmmgt fr 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance 43 #5445: Decane A=,-*A,*,4AMat 10.80 11.00 11.20 11.40 57 m/z 85.10 21.53% 50001 29 71 85

m/z—> m t < 111J ,.. 1.. 199 113 126 ............ ' I ‘ ‘ ‘1T' ‘“1111 > | ■ ■ ■ "j ‘

10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 ‘ ‘ 11 > u I > ‘ f | I I ‘ 11 I I |TTri I I I I I I I I ALA 10.80 11.00 11.20 11.40

11284.D SCAN020507.M Fri May 17 13:06:40 2002 Page 9

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