GCMS results for sample AE08068, Apr 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020415\08068.D Vial: 25 Acq On : 16 Apr 2002 6:25 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 9 Butane, 2,3-dichloro-2-methyl- Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T. 5 : 64 1.58 ug/L 1037040 1,4-Dichlorobenzene-d4 9.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butane, 2,3-dichloro-2-methyl- 140 C5H10C12 000507-45-9 83 2 Butane, 2-chloro-2-methyl- 106 C5H11C1 000594-36-5 39 3 Propane, 2-bromo-1 -chloro- 156 C3H6BrCl 003017-95-6 38 4 1-Propene, 3-chloro- 76 C3H5C1 000107-05-1 18 Abundance Scan 436 (5 641 min) 08068 D (-427) (-) m/z 77.20 100.00% 77

41 5000- 69

53 105 5.20 5.40 ' 5.60 5 80 ' 6 00 89

m/z-> 1 0- 111" " r1 r i 1 „pll $1— 1 11 1 '' I, 125 10 20 30 40 50 60 70 80) 90 100 110 120 130 140 150 160 ' I 1 ' 1 1 ■ i ■ ■ ■ ■ i ■ ■' ■ i111' i'' m/z 41.30 61.68%

k MW Abundance #29395: Butane. 2,3-dichloro-2-methyl- 77

41 5000 5 20 5 40 5 60 5.80 6.00 69 m/z 76.20 39.68% 27 . 53 1 20 105

n/z-> 111111 ■1 c 10 20 1-+414L61TTT .89 97 I, 30 40 50 ' I....... I....... I...... . I 60 70 80 90 100 110 120 130 140 150 160 125 1 140 i ■1111 ■ i ■ ■ ■ > । >

Abundance #108848 Butane. 2-chloro-2-methyl- 41 711 55 1 27 5.20 5.40 5.60 5.80 6.00 5000- m/ z 69.30 34.49% 15 '9 63 91

m/z—> 0- 11111,1 " rrrll. 10 20 30 40 +48450474 0,mm 60 70 80 90 100 110 120 130 140 150 160 ....................... ............................ Abundance #115667 Propane. 2-bromo-1-chloro- 77 5.20 5.40 5 60 5 80 6 00 m/z 79.20 30.91% 5000- 41

27 1 49 63 I -hmPP 93 107 121 129 143 158 0 • ■ i • • • > i ■ > ■11 ■ TIPIPPUTIITTT Tl/Z--> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 5 20 5.40 6 00

08068.D 041202SCAN.M Tue Apr 16 13:56:52 2002 Page 12

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