GCMS results for sample AE08068, Apr 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020415\08068.D Vial: 25 Acq On : 16 Apr 2002 6:25 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 10 2-Butene, 1-bromo-3-methyl- Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

5.70 0.64 ug/L 422412 1,4-Dichlorobenzene-d4 9.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Butene, 1-bromo-3-methyl- 148 C5H9Br 000870-63-3 78 2 2-Methyl-4-bromo-l-butene 148 C5H9Br 020038-12-4 72 3 2-Butene, 1-bromo-3-methyl- 148 C5H9Br 000870-63-3 53 4 2-Butene, 1-bromo-3-methyl-__________ 148 C5H9Br 000870-63-3 50 Abundance Scan 447 (5 706 min)' 08068 D (-441) (-) m/z 69.30 100.00% 4(1 69

5000

53 148 R... M 5 40 5.60 5 80 ■ ' I ' ' '‘I 6.00

n/z-> 0+ ........... I ■ '' ' I' ' "‘I 10 20 30 40 Al... . 88

50 60 70 80 90 100 110 120 130 140 150 A m/z 41.30 96.10% Abundance #2472 2-Butene. 1-bromo-3-methyl-

N.w 41 69

5000 5 40 5.60 5 80 6.00 27 53 m/z 39.30 19.64%

0+ 15 > । i ■ ■■> । । ■11111734.41,11-62. —r 81, . 93 ।, 107 . . 119 . | 133.150, n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #22284 2-Methyl-4-bromo-1-butene 69 41 5.40 5.60 5 80 6 00 5000 m/ z 53.25 15.27% 55 27 148

Tl/Z-> 0+ . 1, 1 ' 11 10 20 30 I 11 l 40) 50 60 —+70 80 90 100 110 120 130 ' I ' ■' ■ I'' ’' I' 140 150 A Abundance #108782: 2-Butene, 1-bromo-3-methyl- 41 69 5 40 5 60 5 80 6.00 m/z 148.20 13.64%

5000 27 53 150 0 ' ' I rnup +3444 4— hit... 15 81 93 107 119 133 TTT n/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 5.40 5.60 5.80 6.00

08068.D 0412 02SC7VN. M Tue Apr 16 13:56:52 2002 Page 13

NYC-WTC_000046829