GCMS analysis results for sample AE07632, April 9, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020415\07632.D Vial: 11 Acq On : 15 Apr 2002 6:58 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 2 Butenol, methyl- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

4.98 0.33 ug/L 244794 1,4-Dichlorobenzene-d4 9.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butenol, methyl- 86 C5H10O 060766-00-9 45 2 Butane, 2-bromo-2-methyl- 150 C5HllBr 000507-36-8 43 3 3-Buten-2-ol , 2-methyl- 86 C5H10O 000115-18-4 38 4 Oxirane, propyl- 86 C5H10O 001003-14-1 38 Abundance Scan 324 (4 983 min) 07632 D (-320) (-) m/z 71.25 100.00% 43 71

5000

53 59 4.4 4.60 4.80 A 5 00 5.20 5.40

Tl/Z--> 01 ■ 1 i ' ' ' 1 i ■ ' ■ ' i 10 20 30 A4l—44MLl 40 50 60 70 - 80 85

90 100 110 120 130 m/ z 43.25 85.67% Abundance #24435: Butenol, methyl- 43 7h

A 44 M moione 5000 59 27 4 60 4.80 5.00 5.20 5.40 15 m/ z 41.25 55.77% 53

n/z-> 0 ' 1 । > l । 1 । ■ । । । 10 20 30 3444 I1, pl, +654441.79.86.. ..... / 40 50 60 70i 80 90 100 110 120 130 Abundance #6326 Butane, 2-bromo-2-methyH 43 71 AKMAMMaA 4.60 4 80 5 00 5.20 5.40 5000- m/ z 69.30 32.67% 27 55 1 n/z- > Ol — 10 15

20 —34 +++ 30 40 50 60 ‘‘‘‘I 70 81 IIIIII 80 90 100 110 121 120 130 Abundance #114556: 3-Buten-2-ol, 2-methyl- 7h 4 60 4.80 ‘IT 5.00 —l 5.20 5 40 43 m/z 59.30 32.38%

5000 59 27 53 —

Tl/Z-> 0 | ii 37 । ,i -ll 1 1 1 1 1 1 1 I ' 1 ' 1 1......... t |ir 10 20 30 40 50 +6544 60 70 ......... 86.............. 80 90 100 110 120 130 - 4.60 4 80 5.00 5 20 540

07632.D 041202SCAN.M Tue Apr 16 13:41:30 2002 Page 5

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