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GCMS results sample AE08258, April 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AE08258 showing surrogate recovery and unknown compounds from April 2002.

NYC-WTC_000047926–000047950

Folder label: “GCMS X 4/8/02 A 4/17/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020417\08258.D Vial: 16 Acq On 17 Apr 2002 9:50 pm Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 10 Octane, 1-chloro- Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 11.03 0.26 ug/L 279924 1,4-Dichlorobenzene-d4 9.99 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Octane, 1-chloro- 148 C8H17C1 000111-85-3 72 2 Octane, 1-chloro- 148 C8H17C1 000111-85-3 72 3 Octane, 1-chloro- 148 C8H17C1 000111-85-3 56 4 Heptane, 1-chloro-________________________ 134 C7H15C1 000629-06-1 40 Abundance Scan 1353 (11.029 mm) 08258.D (-1343) (-) m/ z 91.10 100.00% 91

5000 41 55 69 83 105 ...... B....... I H 10 80 11 00 11 20 11.40

n/z—> 0- —50 + ... 1111111114‘4nuI 11 10 20 30 40 60 70 80 90 m/z 55.10 48.54% 100 110 120 130 140 150 Abundance #117172 Octane, 1-chloro- 9|1 43

55 5000 29 nnt.... J............. 1080 11 00 11 20 11.40 69 m/z 41.10 48.08% 83 105

n/z-> 0- ■ ■ । 10 22 । 11 ■ 1 20 MH 30 40 +T 50 2 76 , 98 1,112119 ' 11 11 ■' 1 ■ i ■ ■' ■ i ■1 ■ ■ i' ■ 60 70 80 90) 100 110 120 130 140 150 148 l 11 11 111

Abundance #117170 Octane, 1-chloro- 9h aMAAAM AAAAA A ,0 AA,. 43 10 80 11 00 11 20 11.40 5000 55 m/z 43.05 43.87% 69 29

mJ 83 105 0- "I’’15.... 1 ’’’’’ 62 176 I,. i +1uT.— +498, 1,112119 148 n/z- > 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #117160 Octane, 1-chloro- .1 rNunaatun) huhhuiiat 4[ 91 _____ 10.80 11 00 11 20 11.40 m/z69.10 30.85% 27 55 5000 69 83 105 Prr i ! I I | ! i r'M 62 I - I, 119 0 +44 1 ' i ■1 ' ■ i ■ ■' ■ i ■' ■ CPPPIMTTI । 11 1 Tl/Z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 10 80 11 00 11.20 11.40

08258.D 041702SCAN.M Thu Apr 18 09:37:43 2002 Page 15

NYC-WTC_000047944

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NYC-WTC_000047944Source: NYC Law Department, mirrored locally

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