GCMS Analysis Results, Sample AE08261, April 22, 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020417\08261.D Vial: 18 Acq On : 17 Apr 2002 11:29 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L ********************************************************************* Peak Number 3 Hexanal Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

5.15 0.31 ug/L 395594 1,4-Dichlorobenzene-d4 9.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexanal 100 C6H120 000066-25-1 46 2 Hexanal 100 C6H120 000066-25-1 46 3 Hexanal 100 C6H120 000066-25-1 43 4 Hexanal 100 C6H120 000066-25-1 43 Abundance Scan 353 (5 153 min) 08261 D (-344) (-) m/z 45.10 100.00% 45 56

5000 129 39 A...................... .. ................. 72 82 1 ■ I 1 1 1 1 I 1 1 r 1 I1 ’ f T-p 11 1 I r

Tl/Z-> 01 P I । I ' । I । । । ' p । I I I vI I . 'll । ■ 10 20 30 40 50 60 III r' I 11 70 80 — .......................... Ill...... 90 ' I 1 ' ' 1 I ' ' ' ' I 1 ' ' ' I ' ' ' ' I ' ' ' 1 I 100 110 120 130 4 80 m/z 5 00 56.10 A 5 20 5.40_______ 85.73% Abundance #110561: Hexanal 41 56

5000 27 mpp 4 80 5.00 5.20 ...... 5.40_______ 72 m/z 44.05 83.03% 82

Tl/Z--> 0+ -4l +14 12,1, 10 20 30 40 50 50 60 70 80 98 ' i ' ■ 1 1 I 1 ' ■ ■ i ' ■ ■ ■ i 1 ' 1 1 i ' 1 ■ 1 I 90 100 110 120 130 Abundance #110563: Hexanal 41 56 werrpatc 4 80 5 00 5.20 5.40_______ 27 5000- m/z 57.00 70.41%

72■ 82

Tl/Z-> 0) ....... 10 1,11371 2030 40 150. 50 +60 +70 80 - 90 100 110 120 130 Abundance 41 56 #110562 Hexanal 4 80 40— 5 00 5 20 5.40_______ m/ z 41.10 67.12%

5000

Tl/Z--> 15 0 T-r-p-Hn-r-r-r 10 20 27

1 4,' 141 „50.1 MX/. । 30 38 I 40 50 60 72

70 82

80 | 90 100 TIBa//—UB3T—EmODTT 100 110 120 130 MMMM "Woryaa 4AA 4.80 5.00 15.20 5.40

08261.D 041702SCAN.M Thu Apr 18 09:47:22 2002 Page 8

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