GCMS results sample AE08258, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\1\DATA\020417\08258.D Vial: 16 Acq On 17 Apr 2002 9:50 pm Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L Peak Number 9 Glycine, N-acetyl- Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 9.84 0.23 ug/L 251152 1,4-Dichlorobenzene-d4 9.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Glycine, N-acetyl- 117 C4H7NO3 000543-24-8 4 2 1,2,5-Oxadiazole 70 C2H2N20 000288-37-9 4 3 Carbamic acid, ethyl-, ethyl ester 117 C5H11N02 000623-78-9 4 4 5-Aminovaleric acid 117 C5H11NO2 000660-88-8 4 Abundance Scan 1150 (9 836 min) 08258 D (-1148) (-) m/z 40.00 100.00% 4b

5000 70 54 45 102 117

n/z-> o1 • 1 I I ' ' ' I ■ 1 1 1 I ■ ' ■ > I ' 10 20 30 40। ll 50 60 • i ■ ■ 70 87 ......... | J......... 80 90 100 110 120 m/z 9.60 70.00 9 80 10.00 10.20 42.39% Abundance #108188 Glycine, N-acetyl- 33 43

5000 9.60 9 80 10.00 10.20 72 15 m/z 54.10 30.43% 1 56 99 117 A Tl/Z--> oJ > i ■ • ■ 1 i ■ 10 20 30 — 40 +50 50 ''-’•I1' . 60 .... 1.77 70 80 84 90 93 | i ■ ■ > ■ । ■ ■ ■ ■ | 100 ■ 110 120 Abundance #1414: 1,2,5-Oxadiazole 43 ................................. .......... 9.60 9 80 10 00 10 20 5000 m/z 56.05 24.64% 28 70

0 ' 1 !■ . ............. —L 4 ■ ■ । ' । । Tl/Z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #108266: Carbamic acid, ethyl, ethyl ester TII-Tmm 33 9 60 9.80 10.00 10 20 m/ z 102.00 19.38% 5000- 72 102 44 88 117

n/z-> 0- .................‘I 10 20 Ho, 38,111,-50, - :30 40 50 58

60 70 81 80 —90 95 — 100 108 । 1 I ' 1 । I । । 1 110 120 ,I 9 60 9 80 10.00 10.20

08258.D 041702SCAN.M Thu Apr 18 09:37:43 2002 Page 14

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