GCMS results sample AE08258, April 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08258.D Vial : 16 Acq On : 17 Apr 2002 9:50 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 8 Boron, trihydro(N-methylmet... Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T.

9.79 0.38 ug/L 411371 1,4-Dichlorobenzene-d4 9.99 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Boron, trihydro(N-methylmethanam... 57 C2H8BN 000074-94-2 37 2 Cycloheptanol, 2-chloro-, trans- 148 C7H13C1O 069578-07-0 35 3 1,2-Cyclopentanediol, trans- 102 C5H10O2 005057-99-8 28 4 Butyl aldoxime, 2-methyl-, syn- 101 C5H11NO 049805-56-3 17 Abundance Scan 1142 (9.789 min): 08258.D (-1137) (-) m/z 40.00 100.00% 4b 56

5000 67 86 47 117 9.40 9.60 9 80 10 00 1020 0- II, . I 1 ' i'1 T-r-p m/z 43.10 100.00% n/z-> 0 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #109528: Boron, trihydro(N-methylmethanamine)-, (T-4)-

WAloon 4 55 28

5000 13 940 9 60 9 80 10 00 10.20

I m/z 56.05 76.39%

n/z- > 0- 0 .. Illl, 231 1.37 +5L 10 20 50 60 30 70 80 40 90 100 110 120 130 ‘ ' i ■ ■ ' ■ i ■ 1 i ■ ‘ 1 ■ i ' ' 1 • i ■ '

Abundance #18516 Cycloheptanol. 2-chloro-, trans- 58 41 68 9.40 9 60 9.80 10.00 10.20 79

P 5000 95 m/z58.10 74.17%

51 113

n/z- > 0- 0 10 20 30 40 50 70 K60m I— 80 90 100 III......110 120 130 130 “PA Abundance #14366 1.2-Cyclopentanediol. trans- i 1 1 ■ ' । ■ 55 9 40 9 60 9 80 10 00 10 20 m/z 55.00 69.58% 84 41 5000

. 69 n/Z- > 0- 0 . ........... WUh. +l 10 20 30 40 50 60 70 80 100 ' I ' ' ' ' I 1 ' ' ' I ' 1 ' ' I ' ' ' ■ I ' ‘ 90 100 110 120 130 2/111104 . 9.40 9 60 9.80 10.00 10.20

08258.D 041702SCAN.M Thu Apr 18 09:37:43 2002 Page 13

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