GCMS analysis results for sample AE08251, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08251.D Vial: 9 Acq On : 17 Apr 2002 4:02 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L

Peak Number 8 Boron, trihydro(N-methylmet... Concentration Rank 18

R.T. EstConc Area Relative to ISTD R.T. 4.89 0.24 ug/L 224181 1,4-Dichlorobenzene-d4 9.99

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Boron, trihydro(N-methylmethanam... 57 C2H8BN 000074-94-2 9 2 Pyrrolidine, 3-methyl- 85 C5H11N 034375-89-8 5 3 Diazene, dimethyl- 58 C2H6N2 000503-28-6 5 4 Acetone 58 C3H60 000067-64-1 5 Abundance Scan 307 (4 883 min) 08251 D (-303) (-) m/z 43.00 100.00% 43

5000

0- • i ■ ■ • ' i 1 ' i ■ T 49 58 85 . . . AN w . 4.60 m/z 4 80 58.00 5.00 5 20 51.06% n/z—> 0 10 20 30 40 50 60 70 80 90 100 Abundance #109528: Boron, trihydro(N-methylmethanaminej-, (T-4)-

28 43 55

5000' 11 13 4 60 4.80 5.00 5.20 38 m/z 40.00 46.63%

n/z- > 0- 0 —1) - 10 i 20 231 30 | - 40 —l 50 'i 1 1 1 1 i 1 60 70 80 90 100 Abundance #7036: Pyrrolidine, 3-methy- 43 4.60 4 80 5.00 5 20 5000 m/z 57.10 37.79% 85 } 28

o- -1520,133 34,1 80 —| * , 91 , 51 56 61 TH68t-i 7. 5. Id 1 ' 1 ’ll’ I I ' । , n/z-> Abundance 0 10 20 30 40

15 50 60 80 90 #6. Diazene, dimethyl- 70 100

4.60 7 4 80 5 00 5.20 43 m/z 85.00 29.95% 5000 28 58

n/Z-> 0— 0 -4 — 10 20 +30 40 ' I ' 50 60 70 80 90 100 4 60 4.80 5.00 5.20

08251.D 041702SCAN.M Thu Apr 18 09:12:14 2002 Page 13

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