GCMS results sample AE08258, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08258.D Vial : 16 Acq On : 17 Apr 2002 9:50 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L ********************************************************************* Peak Number 7 3-Pentanol, 2-methyl- Concentration Rank 14

R.T. EstConc Area Relative to ISTD R.T.

9.71 0.21 ug/L 229929 1,4-Dichlorobenzene-d4 9.99

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 2-methyl- 102 C6H140 000565-67-3 12 2 Propane, 1-ethoxy-2-methyl- 102 C6H140 000627-02-1 9 3 3-Hexanol, 4-methyl- 116 C7H160 000615-29-2 9 4 Silane, ethyldimethyl- 88 C4H12Si 000758-21-4 9 Abundance Scan 1129 (9 713 min) 08258 D (-1125) (-) m/z 59.05 100.00% 59 1 40 86 103 5000 47 73

9.40 . Mll 9 60 9.80 10.00 04 । * •• « । * m/z 103.10 50.19% Tl/Z-> 0 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #113304: 3-Pentanol, 2-methyl- 59

5000- 41 73 9.40 |k 9 60 9.80 10.00 18I

31 m/z 86.10 49.94% 251,,. „11 r5l _W 67 84 100 0- i ■ ■ ■ ■ i ■ ' I ' ' ''ll1 ■ ■ । > । । 1 , i i i ... । . i i i | i r n/z-> 0 10 20 30 40 60 50 70 80 90 100 110 120 Abundance #113141: Propane, 1-ethoxy-2-methy- 59 31 9.40 9.60 9 80 10.00 5000 m/z 40.00 49.56% 41 15 73 102

n/z-> 04 2 ' ' I ' 1 ' ' I 0 10 125144447,531 1 20 30 40 50 60 70 | 79 87 । > । 1 ■ ■ । । 1 ■ ■ ■ । ■ ■ ■ ■ । l 1 । ' I 1 1 1 > I > 1 80 90 100 110 120 Abundance #113235: 3-Hexanol, 4-methyl- 59 940 9 60 9.80 10.00 m/z 45.05 38.81% 5000 31 45

69 87 39

n/z—> 0 0 I 1 1 1 1 1 1 10 15 —254—44 ,53 — 20 30 40 50 60 70 77| 80 90 98 100 110 115 120 9 40 9 60 9.80 10 00

08258.D 041702SCAN.M Thu Apr 18 09:37:43 2002 Page 12

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