GCMS analysis results, Sample AE08266, April 22, 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08266.D Vial : 23 Acq On : 18 Apr 2002 3:33 am Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L Peak Number 4 3-Pentanol, 3-methyl- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

5.97 0.40 ug/L 480910 1,4-Dichlorobenzene-d4 9.99 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 28 2 Acetic acid, 3- [1,3]dioxolan-2-y. .. 174 C8H14O4 1000186-02-3 28 3 1-Propene-l-thiol 74 C3H6S 000925-89-3 25 4 Silane, tetramethyl-88 C4H12Si 000075-76-3 25 Abundance Scan 492 (5.970 min): 08266.D (-487) (-) m/ z 73.10 100.00% 73

5000 43

5.60 5 80 6 00 6.20 6.40 । I 55 87 103 0+ ■ r ' " r " ' i1 10*0u—uunmNT m/z 43.10 30.26% n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #114875 3-Pentanol. 3-methyl- 73

5000 5 60 5.80 N 6.00 k 6.20 6.40 55 m/ z 45.10 11.23% 27 45 87

n/z-> 15.41371 +3— 4 I’l 11111*111011111111011*11/0000100002*0// T’T o TITT।'11111 ‘11. . . ....... ... 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #25344 Acetic acid, 3-[1.,3]dioxolan-2-ylpropyl ester 73 5 60 5 80 6.00 6.20 6.40 5000- m/z 41.10 9.56% 43 27 55 87 113 131 174 0) ' ।11 1111 ' 1h* ।' ''i'l , i TIT 11'" ■ ।1" ' i1 ■■I 1' l1 ■ ■ > I' > > • l i " " r " ■ i ■1 ■ ' i " wz-> Abundance 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 #25348 1-Propene-1-thiol ahudojsaaap.Vuajaomusas 73 5 60 5 80 6 00 6.20 6.40 m/z 71.00 7.00% 5000 43

ill, 55 65 , 0 ‘ I " " 111" i1" ri 11’di’l’i । " ' 11 Tl/Z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20 6.40

08266.D 041702SCAN.M Thu Apr 18 09:59:57 2002 Page 9

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