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GCMS analysis results, Sample AE08266, April 22, 2002

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GCMS analysis report for sample AE08266 showing surrogate recovery and unknown compound screening on April 22, 2002.

NYC-WTC_000048401–000048420

Folder label: “GCMS X 4/9/02 A 4/17/02

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Scanned page image, NYC-WTC_000048414
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08266.D Vial: 23 Acq On : 18 Apr 2002 3:33 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 5 2-Propanone, 1,1,1-trichloro- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

6.04 0.81 ug/L 960529 1,4-Dichlorobenzene-d4 9.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 40 2 N-(2-Mercaptoethyl)-acetamide 119 C4H9NOS 1000194-02-5 9 3 .beta.-d-Fructofuranose, 1,3,4-t... 288 C12H1608 1000151-08-8 9 4 Tetrahydropyrrole-3-ol-5-carboxy... 187 C8H13N04 1000128-67-1 9 Abundance Scan 503 (6.035 min): 08266.D (-498) (-) m/ z 43.05 100.00% 43

5000 NV —TT-PTTTTTTTTTT 83 97 125 5.60 5.80 6.00 6.20 6.40 i 59 th h|i . ।. Il. । । .... 1__|__ | ' m/z 124.90 10.37% 01 1 1 i 1 1 1 n* ' 1 1 r Tl/Z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #3877 2-Propanone, 1,1,1-trichloro- 43

........................ ............................... 5000 5.60 5.80 6.00 6 20 6.40 m/z 47.00 6.87% 01 15 27 +6.2,7 . ................. . -++ _ n/z- > 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #747: N-(2-Mercaptoethyl)-acetamide 33 43 60

5.60 5 80 6.00 6.20 6.40 5000 m/z 83.0.0 6.46%

J 72 101 119 ■n/z-> 01 1444 ’ ‘ I ' 1 20 40 60 . 80 86. -L

100 I •

120 140 160 - i—i—i—r _

180 . 200 —i—i—i—i ■

220 —i—i—r

240 Abundance #6136: beta.-d-Fructofuranose. 1,3,4-tri-O-acetyF2.6-anh... |.. At | it ..... 43 5.60 5.80 6.00 6.20 6.40 m/ z 97.00 6.24% 5000

69 0 101 — 128 29 0 ■ i ■ r* ■ i 1 57 1 “i . 115 . .. 145 157 170 187 203 215 229,245 n/z—> 20 40 60 80 100 120 140 160 180 200 220 240 5.60 5 80 600 6 20 6.40

08266.D 041702SCAN.M Thu Apr 18 09:59:57 2002 Page 10

NYC-WTC_000048414

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NYC-WTC_000048414Source: NYC Law Department, mirrored locally

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