GCMS results for sample AE08069, Apr 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020415\08069.D Vial: 26 Acq On : 16 Apr 2002 7:13 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C: \MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 4 2-Propanone, 1,1,1-trichloro- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 6.03 0.66 ug/L 455589 1,4-Dichlorobenzene-d4 9.98

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

7 1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 72 2 N-(2-Mercaptoethyl)-acetamide 119 C4H9NOS 1000194-02-5 9 3 N-Acetylpyrrolidone 127 C6H9NO2 000932-17-2 5 4 2-Acetylthiazole 127 C5H5NOS 024295-03-2 5 Abundance Scan 501 (6 023 min): 08069.D (-496) (-) m/z 43.25 100.00% 43

5000

5 60 5 80 6 00 6 20 6 40 01 35 . ,19 63 83. 97 119125 ' 1 I ' 1 ' ' I ' ' ' ' 1 1 ,,'‘l l ' 1‘11tt111*/+/1/1/11/*/1/1/1/1//r/r1/*/r*/*11/1/11/1/*1/1/1/1/1//1/1/T m/z 125.10 9.59% n/z-> Abundance 10 20 30 40 50 60 70 80 90 100 #3877 2-Propanone, 1.1,1-trichloro- 110 120 130 ft 43

5000 5 60 5 80 6.00 6 20 6.40 m/z 127.20 6.98% 15 | 27 36 49 55 63 76 83 91 97 110 117 125 01 ■ > । ■ i ■ > । ■ 111 । ■ I’i । । n/z- > 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance . N-(2-Mercaptoethyl)-acetamide 3b 43 60

5 60 5 80 6.00 6 20 640 5000 m/ z 97.20 6.69%

72 0- ’ ' i ' 1 ■ ■ i ■ —4 11—54. 4 11 178' 1 1 '''861 l ' 9511 '101orn 1 I '-n-iT' 119 i■■ । ■i 71/Z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #7671: N-Acetylpyrrolidone 1 ' 1 1 1 ' 1 I ' ' 43 5 60 5.80 6.00 6.20 640 m/ z 83.20 6.19% 5000 99 127 28 56 86 0 10110111.,37 . —l. ,, ..... II.,90 I7 112 T-r-p-T-T-r-p-r-A-p-r n/z—> 10 20 30 40 50 60 70 80 100 110 120 130 5.60 5 80 6.00 6.20 6.40

08069.D 041202SCAN.M Tue Apr 16 13:58:30 2002 Page 7

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