GCMS results for sample AE08068, Apr 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\1\DATA\020415\08068.D vial: 25 Acq On 16 Apr 2002 6:25 am Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L Peak Number 7 2-Pentanol, 3-methyl­ Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 5.13 1.06 ug/L 698218 1,4-Dichlorobenzene-d4 9.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanol, 3-methyl- 102 C6H140 000565-60-6 53 2 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 47 3 Butane, 1-methoxy- 88 C5H120 000628-28-4 40 4 Butane, 1-methoxy-_________________________ 88 C5H120 000628-28-4 40 Abundance Scan 349 ( 5 1 30 min): 08068 D (-343) (-) m/z 45.30 100.00% 45 1 5000 56 69 129 4.80 5.00 5.20 5.40 । 79 87 01 —IPPTTTTT ++H 1i''1'I'-H+ 3^i! i ■ ■ ■ ■ i ■. ■. i II, T’IT 150 IT -7" "I m/z 41.25 33.66% n/z- > 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #11500: 2-Pentanol, 3-methy- 45

5000 —au)Ili or , 1**7 4 80 5 00 5.20 5.40

29 56 m/z 44.25 32.33%

n/z--> ol 11151111077.28 1 ill 69 87 I' F** ■ ’ ' 1 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 । . r.', । । । । । । । । । ।

Abundance #110825: 2-Pentanol, 4-methyl- 45 nanceoeCNupapu 4 80 5 00 5.20 5.40 5000 m/z 43.30 24.69%

69 I 57 87

n/z-> ol ■ ■ । • 10 20 19.,27,.38, P r. I-'1' 94 101 30 40 50 60 70 80 ’90 100 110 120 130 140 150 Abundance #110866. Butane, 1-methoxy- -0" I ' 1 45 4 80 500 5 20 5.40 m/ z 56.30 22.21% 5000

56 20

Tl/Z--> 0 4438, 15 ■ i ■'.. । . 10 20 30 40 50 71 78 88 i' i1 ■ ‘ ‘I ■ ■ ■ ■ | • l 1 • ( > ' ' I | • 1 ' > | 1 ■ ■ l |"l >•! I | I , I , | I I I I | I I 1 I J I I I I | 60 70 80 90 100 110 120 130 140 150 A —

4.80 5 00 5.20 5.40

08068.D 041202SCAN.M Tue Apr 16 13:56:51 2002 Page 10

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