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GCMS analysis results for sample AE07979, Apr 2002

Machine-extracted title · confidence 100%

Laboratory report documenting the GCMS analysis of sample AE07979 including surrogate recovery data and unknown compound screening on April 18, 2002.

NYC-WTC_000046722–000046739

Folder label: “GCMS X 4/5/02 A 4/16/02

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Scanned page image, NYC-WTC_000046733
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020415\07979.D Vial: 19 Acq On : 16 Apr 2002 1:32 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 5 Acetic acid, 3-[1,3]dioxola.. . Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

5.96 0.40 ug/L 311442 1,4-Dichlorobenzene-d4 9.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetic acid, 3-[1,3]dioxolan-2-y. . . 174 C8H14O4 1000186-02-3 36 2 1-Propene-l-thiol 74 C3H6S 000925-89-3 9 3 N-Ethylformamide 73 C3H7NO 000627-45-2 9 4 Butane, 2,3-dimethoxy-2-methyl -____ 132 C7H1602 074421-00-4 9 Abundance Scan 491 (5 964 min) 07979.D (-483) (-) m/z 73.30 100.00% 73

5000- 43 55 . 87 103 5 60 5 80 6 00 6.20 6.40

n/z- > 0- yoospoasgun — Bungatn-outI ■ . I 1. 1’’ 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 1111' I m/z 43.25 24.10% Abundance #25344: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73

5000 5 60 5 80 6 00 6.20 6 40 43 m/z 41.30 10.38% 27 6 1111 " 111 1 --- 55 67.............. 113....... 131............................. 174 I n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #25348 1-Propene-1-thiol 73 MMAt । ■*. -M 5.60 5 80 6 00 6 20 6.40 5000 m/z 45.30 8.46% 43

nil ' I AI 0 1 1 I ' ' 1 ' I ' ' " I 1 1 ' ’ll 65 1, 1 55 .) n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #857 N-Ethylformamide ............ ........................................ 3D 5.60 5.80 6.00 6 20 6.40 73 m/z 71.30 7.33% 5000 44 58 18 0— Tl/Z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5 60 5 80 6.00 6 20 6 40

07979.D 041202SCAN.M Tue Apr 16 13:48:31 2002 Page 8

NYC-WTC_000046733

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NYC-WTC_000046733Source: NYC Law Department, mirrored locally

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