GCMS analysis results, Sample AE08264, April 22, 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08264 .D Vial: 21 Acq On : 18 Apr 2002 1:56 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 2 Chloroform Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

3.39 0.26 ug/L 306110 1,4-Dichlorobenzene-d4 9.99

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Chloroform 118 CHC13 000067-66-3 86 2 Methane, bromodichloro - 162 CHBrC12 000075-27-4 83 3 Chloroform 118 CHC13 000067-66-3 78 4 Chloroform 118 CHC13 000067-66-3 72 Abundance Scan 52 (3.385 min)' 08264.D (-47) (-) m/z 83.00 100.00% 83

5000

47 „ 129 3 20 3 40 3.60 3.80 0+ 111111 111' " l1 37 I i'11’] r"'r H 191.......... r.............. m/z 85.00 59.56% ■n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #33238: Chloroform 83 .... .......................... 5000- 47 3 20 3.40 3 60 3.80 35 m/ z 47.00 20.42%

n/z-> 0 27 " r " 1 r ' " i1 10 20 30 pal50—. 116060 M794 40 ’ | 96 118 11111 l111' I' rrtt’ 111111 ।11'1'11 ■' " i1'1 ■ i'' 70 80 90 100 110 120 130 140 150 160 170 Abundance #33236: Methane, bromodichloro- 83 W 3 20 3.40 3.60 3.80 5000- m/ z 48.00 14.44% ft WA 47 129

n/z-> 13 0+ " ।■11 ■ 27,3%.,.h. 3 11663 72 ll. 164 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 11 " " I' " ' i " ■11 ■ ■ '111 " ■ i " " i'11 ■ i " voyo Wy Abundance #116499 Chloroform 83 3 20 340 3.60 3.80 m/z 128.90 10.14% 1 5000-

47 35 118 Tl/Z—> 0 9 I". . ..... dr..... ri . 7 — 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 i ■' rfl ' । < 111 ■ । > । ■ । > 111 ■ ■ ■ [' '! ■ । . 3.20 3.40 3 60 3.80

08264.D 041702SCAN.M Thu Apr 18 09:52:44 2002 Page 7

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