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GCMS analysis results, Sample AE08264, April 22, 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AE08264 showing surrogate recovery and unknown compound screening on April 22, 2002.

NYC-WTC_000048355–000048377

Folder label: “GCMS X 4/9/02 A 4/17/02

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Scanned page image, NYC-WTC_000048364
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C : \MSDCHEM\1\DATA\020417\08264.D Vial: 21 Acq On : 18 Apr 2002 1:56 am Operator: Nefliu Sample : sample Inst Instrumen ■Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 1 Hexane, 3-ethyl-2,5-dimethyl- Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

3.16 0.31 ug/L 369453 1,4-Dichlorobenzene-d4 9.99

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Hexane, 3-ethyl-2,5-dimethyl- 142 C10H22 052897-04-8 33 2 Hexane, 2,2,3-trimethyl- 128 C9H20 016747-25-4 25 3 Hexane, 2,2,5-trimethyl- 128 C9H20 003522-94-9 25 4 Azetidine, 1-methyl- 71 C4H9N 004923-79-9 12 Abundance Scan 13 (3.156 min). 08264.D (-4) (-) m/z 57.10 100.00% 57

5000 43 ' I ' ' ' ' I ' 1 ' ' I 71 86 100 3 20 3.30 340 3.50 3.60 120. 301440 H — 01 ’ i 1 ' 1 ■ I ' 1 1 1 i ■ ■ ■ 1 i 1 ' 1 ' i ■ ■ ■ ■ i ■ 1 ■ ' i m/z 43.05 22.27% n/z-> 50 60 70 80 90 100 110 120 130 140 Abundance #16264 Hexane, 3-ethyl-2,5-dimethyl- 57 W 43 5000 3.20 3.30 3.40 ' 3.50 3.60 m/ z 41.05 17.67% 29 71 r 98 01 .37 +51 65 1177 85 91 /.. 113 142 n/Z-> 20 30 40 60 70 80 90 100 110 120 130 140 50 Abundance

Mywo #16845: Hexane, 2.2,3-trimethyl- 57 3.20 3.30 3.40 3.50 3.60 5000 m/z56.10 15.70% 41 29 71 51 ,| ,'I 1 65 J 77 85 91 97 113 128 0+ - -- TIuk 1 । i | n'i i । i । i >-p i ■ i । ।11 । । . . . . ( ■ . . . । . j __ n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #112488: Hexano, 2,2,5-trimethyl- 57 3.20 3 30 -. -4 3.40 3.50 3.60 m/ z 71.10 14.98%

5000

41 71

Tl/Z--> 0- 29 1, . 1 20 lL 30 40 I 1 ■ 50 + 60 i 70 '‘I 1 1 1 1 1 1 1 ' 1 1 1 1 1 1 I ' 1 ' 1 1 ''' 1 1 1 1 1 ■ ■ i ■ 1 ' ■ i ■ ' 1 1 i 80 90 100 110 113 120 130 140 4. a 3.20 3 30 3.40 3.50 3.60

08264.D 041702SCAN.M Thu Apr 18 09:52:44 2002 Page 6

NYC-WTC_000048364

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NYC-WTC_000048364Source: NYC Law Department, mirrored locally

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