GCMS analysis results, sample AE09331, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\050902\9331.D Vial: 21 Acq On : 10 May 2002 8:24 am Operator: Mclean Sample : 5/8 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHCDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 1 Chloroform Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

3.38 0.42 ug/L 523176 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Chloroform 118 CHC13 000067-66-3 78 2 Chloroform 118 CHC13 000067-66-3 64 3 Methane, bromodichloro- 162 CHBrC12 000075-27-4 59 4 Chloroform 118 CHC13 000067-66-3 56 Abundance Scan 51 (3.379 min): 9331 .D (-45) (-) m/z 83.00 100.00% 83

5000

47 -T-I— — 129 320 3.40 3.60 3.80 O+ 41 5 90 S100 110 120 130 m/z 85.00 71.09% mtz-> 20 30 40 50 60 70 80 Abundance #116499: Chloroform 83

5000 ror 1 PrI । 111111 ।" 3 20 3.40 3.60 3.80 47 m/z 47.10 17.53%

n/z-> 01 ..... 20 135,41.hlp 30 40 50 1111170 60 70 . Prrl 80 | 90 118 100 110 120 130 1 1 I ' ' 1 1 1 1 1 ' 1 1 1 ■ ill । ... । . i . । ।

Abundance #33238: Chloroform 83 320 3.40 3.60 3.80 5000 m/z 48.05 12.94% 47 35 28 O+ ■ - i * > ■ ■ i ■ 141 1—— 63 70 41 | ■ I । * < i l • । ■ I I 96 1 ■ i ■ 1 ■ ' i ' 1 ■ ■ I ' 1 118124 I ' ‘ ■ ■ i ■ ' ' ' i m/z- > 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #116497: Methane, bromodichloro- 83 3.20 3.40 3.60 3.80 m/z 87.00 11.16%

5000

47 129

m/z-> 0 ... 7,135....1........... 1,1.1. 90 100.... 20 30 40 50 60 . I,. 110 120 130 70 80 I 91 11 |rI1! । 3.20 3.40 3.60 3.80

9331.D 050102.M Mon May 13 11:42:31 2002 Page 4

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