GCMS sample results AE11284, DEP Labs, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\02051611284.D Vial: 12 Acq On : 16 May 2002 8:14 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 5 Benzene, 1,2,3-trimethyl- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 10.79 1.14 ug/1 65490 1,4-Dichlorobenzene-d4 11.37 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzene, 1,2,3-trimethyl- 120 C9H12 000526-73-8 95 2 Benzene, 1,2,4-trimethyl- 120 C9H12 000095-63-6 94 3 Benzene, 1,2,3-trimethyl- 120 C9H12 000526-73-8 91 4 Benzene, 1,3,5-trimethyl-__________ 120 C9H12 000108-67-8 91 Abundance Scan 1313 (10.794 min): 11284.D (-1305) (-) m/z 105.10 100.00% 105

5000 120

39 , 51 57 65 77 1, 83 I 4 Y ...... AY.,...... 10.40 10.60 10.80 11.00 11.20 .7 i , 11110411 i1.1! i । ■ , eili I'I I 11 alai j_______ ‘I m/z 120.10 37.75% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #46796: Benzene, 1,2,3-trimethyl- 1(6

5000 120 V .... ................... 10.40 10.60 10.80 1100 11.20 m/z 77.10 14.54% _ 27 39 51 e 77 91 A m/z-> — 10 154655859 20 30 40 50 60 70 80 +1141— 90 100 110 120 1II

Abundance #46773: Benzene, 1,2,4-trimethyl- 1(6 i ■ 1 ■ ■ i ■ —44 10.40 10.60 10.80 11.00 11.20 5000, 120 m/z 119.10 10.95% 28 91

niz-> 14 J 30,45 51.585.7 85,498-4——ul 11 i' 1 1 1 i ■ ■ 1 ' i ■ . ‘*.4 . . . p, . i । ri'i । । i rrr| ! 10 20 30 40 50 60 70 80 90 100 110 120 TI

Abundance #119303: Benzene, 1,2,3-trimethyl- 1(6 10.40 10.60 10.80 11-00 11.20 m/z 91.10 1 10.27% 15 120 5000

/z—> —15774515 55. 44..71,97,4 +111444 10 20 30 40 50 60 70 80 90 100 110 120 ‘II 10.40 10.60 10.80 11.00 11.20

11284.D SCAN020507.M Fri May 17 13:06:39 2002 Page 8

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