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GCMS results for sample AE11427, May 29, 2002

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Laboratory report of GCMS analysis for sample AE11427 conducted on May 29, 2002.

NYC-WTC_000022550–000022560

Folder label: “GCMS X 5/17/12 A 5/21/02

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NYC 9/11 Public Portal Document LIbrary Search Compound Report Data File : C:\MSDCHEM\1\DATA\020521\11427.D Vial: 13 Acq On : 21 May 2002 8:13 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 Benzene, 1,4-bis(dichlorome... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 28.90 0.21 ug/1 21719 Phenanthrene-dl0 31.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Benzene, 1, bis(dichloromethyl)- 242 C8H6C14 007398-82-5 28 2 Benzene, 1, 3,5-tetrachloro-4, 6... 242 C8H6C14 000877-09-8 16 3 Benzoic aci 2,4,6-trichloro- 224 C7H3C13O2 000050-43-1 12 4 5,7-Dioxooctanoic acid 172 C8H12O4 1000099-93-6 9 Abundance Scan 4395 (28.902 min): 11427.D (-4385) (-) m/z 206.90 100.00% 207

5000 86 50 137 172 242 | I | 476 28.60 28.80 29.00 29.20 OTT m/z 209.00 72.19% nz-> 0 50 100 150 200 250 300 350 400 450 Abundance #84882: Benzene, 1,4-bis(dichloromethyl)- 172 207

5000 101 28,60 28.80 29.00 29.20 51 75 m/ z 85.80 40.78%• 1 137 244 /z—> 0 ,ob 27 * r 50 +4100— —— 150 , , 1" , 1, , , . .. 1 200 250 300 350 400 450 Abundance #84890: Benzene, 1,2,3,5-tetrachloro-4,6-dimethyl- 207

244 28.60 28.80 29.00 29.20 5000 m/z 49.80 35.76% 136 51 85 i 171 OTT ... x.1,h,4 4 09 4—— Z—> 0 50 100 150 200 250 300 350 400 450 Abundance #126482: Benzoic acid, 2,4,6-trichloro- ............ 1....... 1 । 1 1 ■ ■ । ■7 1 ■ । ■ ■ i ■ ‘ ' i 207 28.60 28.80 29.00 29.20 74 m/z 171.90 33.87% 5000 109 45 144 179 2 28 0| 74444 4u 4k r . li,. z— > 0 50 100 150 200 250 300 350 400 450 28.60 28.80 29.00 29.20

11427.D SCAN020521.M Fri May 24 09:30:35 2002 Page 4

NYC-WTC_000022557

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NYC-WTC_000022557Source: NYC Law Department, mirrored locally

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