GCMS analysis results, sample AE11157, May 22, 2002

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Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\020515\11157.D Vial: 9 Acq On : 15 May 2002 7:43 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 4 Benzene, 1,2,3,5-tetrachlor... Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 28.90 0.23 ug/1 . 25475 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Benzene, 1,2,3,5-tetrachloro-4,6... 242 C8H6C14 000877-09-8 22 2 2,3,6-Trichlorobenzoyl chloride 242 C7H2C14O 004093-17-8 12 3 7-Chloro-4-methoxy-3-methylquino. . . 207 C11H10C1NO• 1000213-52-2 10 4 Ethanone, /I-(2,3,4-trichlorophen... 222 C8H5C13O 013608-87-2 10 Abundance / Scan 4395 (28.902 min): 11157.D (-4383) (-) m/z 209.00 100.00% 209

244 5000 49

i 85 137 1 i 172 LL41091 | ITT ............................................................ 520 28.60 28.80 29.00 29.20 m/ z 2 07.00 98.62% m/z-> 50 100 150 200 250 300 350 400 450 500 Abundance #84890: Benzene, 1,2,3,5-tetrachloro-4,6-dimethyl- 207

244 5000 0 1 1 136 28.60 28.80 29.00 29.20 85 m/z 243.90 52.03%

mlz-> A 4 50 51 , ।

100 09 — 150 171

200 250 300 350 400 450 500 Abundance #84883:2,3,6-Trichlorobenzoyl chloride 207 • ■ । । I । ■ ■ । I 28.60 28.80 29.00 29.20 5000 m/ Z 49.05 47.14% 74 179 37 i 109 143

MMAWhMM 244

m/z-> -,4444444 1, 50 100 150 200 250 300 350 400 450 500 V Abundance #84815:7-Chloro-4-methoxy-3-methylquinoline 207 28.60 28.80 29.00 29.20 178 m/z 84.90 36.35% 75 5000

51 102 138

m/z—> LMnlal J 4 1 +lu TT 50 100 150 200 250 300 350 400 450 500 JU 28.60 28.80 29.00 29.20

11157.D SCAN020507.M Thu May 16 09:38:57 2002 Page 6

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