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GCMS sample results AE11284, DEP Labs, June 2002

Machine-extracted title · confidence 100%

Gas chromatography mass spectrometry results for sample AE11284 analyzed on June 4, 2002.

NYC-WTC_000014781–000014806

Folder label: “GCMS X 5/29/02 A 5/30/02

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\020516\11284.D Vial: 12 Acq On : 16 May 2002 8:14 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library . : C:\DATABASE\nist98.I ********************************************************************* Peak Number 4 Benzene, 1,3,5-trimethyl- Concentration Rank 19

R.T. EstConc Area Relative to ISTD R.T. 9.87 0.60 ug/1 34073 1,4-Dichlorobenzene-d4 11.37 Hit# of 5 Tentative ID MW MolForm CAS# Qual

l Benzene, 1,3,5-trimethyl- 120 C9H12 000108-67-8 22 2 Benzene, 1-ethyl-4-methyl- 120 C9H12 000622-96-8 14 3 2,4-Nonadiyne 120 C9H12 063621-15-8 14 4 Benzene, (1-methylethyl) -________120 C9H12 000098-82-8 14 Abundance Scan 1155 (9.865 min): 11284.D (-1147) (-) m/z 57.20 100.00% 57 1(6

J 43

5000 70 120 AAA I 83 81 7ifz-> ••। > i»» +lu444 4 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 180 9.60 m/z 105.05 9.80 10.00 10.20 99.79% Abundance #119302: Benzene, 1,3,5-trimethyl-

5000

27 39 51 65 79 91 105

120 _. W N m/z 9.60 9.80 43.10 10.00 10.20 78.96%

miz—> ----- —Lmmmmmm 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #119288: Benzene, 1 -ethy-4-methyl- 105 9.60 9.80 10.00 10.20 5000 m/z41.05 48.81% 120 77 91 2 39 51 65 li I miz-> -HH# I,■................. ....................... ‘ ‘11.1.1.1‘* ‘‘‘‘I ITT4 j. 1. 11.1111111J11. H11».. 10 20 30 40 50 60 70 80 90 100 110120 130 140 150 160 170 180 Abundance #45884:2,4-Nonadiyne MAAAAM , 105 9.60 9.80 10.00 10:20 m/z 70.20 42.98%

5000 77 120 39 51 63 miz—> 15 27 91 m ,11|.. I'lrr,l p-r., o , u । I r ..,11 rr, ..., |। m M ...+ । ,L ।। 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 J *i 11111 i 11111 r 11 > 111111111 111111111 AALLAALN 9.60 9.80 10.00 10.20

11284.D SCAN020507.M Fri May 17 13:06:39 2002 Page 7

NYC-WTC_000014789

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NYC-WTC_000014789Source: NYC Law Department, mirrored locally

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