GCMS analysis results for sample AE09571, May 2002

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Laboratory report detailing gas chromatography mass spectrometry analysis of sample AE09571 conducted on May 14, 2002.

NYC-WTC_000023023–000023054

Folder label: “GCMS X 5/8/02 A 5/9/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\1\DATA\050902\9570 .D Vial: 7 Acq On 9 May 2002 8:10 pm Operator: Mclean Sample 5/8 kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 3 Tridecane, l-iodo- Concentration Rank 15 R.T. EstConc Area Relative to ISTD R.T. 27.17 1.50 ug/L 2605030 Chrysene-dl2 30.81 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tridecane, 1-iodo- 310 C13H27I 035599-77-0 27 2 Eicosane, 10-methyl- 296 C21H44 054833-23-7 27 3 Pyrene 202 C16H10 000129-00-025 4 Fluoranthene 202 C16H10 000206-44-0 25 Abundance Scan 4099 (27.163 min): 9570.D (-4087) (-) m/z 57.15 Z00.00% 57 /

202 5000 43 71 85 "113 ,151 . , 26.80 27.00 27.20 27.40 27.60

miz-> O-20M il4lL5.—- I I l

40 60 80 100 120 140 160 180 200 220 240 260 280 300 13. I 163 m/z 202.10 63.69% Abundance #16508: Tridecane, 1-iodo 57 43 71 5000 85 26.80 27.00 27.20 27.40 27.60 28 m/z 71.10 47.34% 0-l—l — , ,J,. L 99L 113127141155 183 n/z-> Abundance 20 40

43 57 60 I 111’ ’l ! IT’ | I I I I | I I I 1 | I ! I I | I I I -1 ■ - ■ ■ । 80 100 120 140 160 180 200 220 240 260 280 300 #16468: Eicosane, 10-methyl- 310 • i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ • -11 ■ ■ ■

_MMaar 71 26.80 27.00 27.20 27.40 27.60 5000 85 m/z 43.20 44.51%

99 113 154168 WnAAAunudl O-TTT —A+ J 1 127 ' 'I ' 'T' | h '7’183197211225239253267281295 ’ ’’’ ’ | . I' | I I | I I I I | l-l-i ! | । I I I | I I I । | I I I 1 | I I WWW niz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #126278: Pyrene 202 26.80 27.00 27.20 27.40 27.60 m/z 85.10 31.10% 5000 101 WMWMaopr 29 51 67 87 123 150 174 0- IMi l .......-1 T4 , ’ 11,1, ,■ । r* ■ ।" ।, । 11 ■ ■ । ■1 ■ ■ । ■1 ■ ‘ । ■ ■1111111111 /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 26.80 27.00 27.20 27.40 27.60

9570.D 050102.M Mon May 13 11:46:45 2002 Page 9

NYC-WTC_000023036

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