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GCMS analysis results, sample AE07516, April 2002

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Laboratory report documenting GCMS analysis of environmental sample AE07516 conducted on April 11, 2002.

NYC-WTC_000047389–000047401

Folder label: “GCMS X 4/2/02 A 4/4/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\020404\07516.D Vial: 12 Acq On 4 Apr 2002 5:13 pm Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 5 2-Propenoic acid, n-pentade... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 37.71 1.46 ug/1 1665990 Chrysene-dl2 39.10

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propenoic acid, n-pentadecyl e... 282 C18H3402 1000245-64-0 87 2 Dodecyl acrylate 240 C15H2802 002156-97-0 59 3 5-Octadecene, (E) - 252 C18H36 007206-21-5 58 4 1-Octadecene 252 C18H36 000112-88-9 58 Abundance Scan 5894 (37.710 min): 07516. D (-5882) (-) m/ z 55.10 100.00%

43 5000 69 83 97

0* । । > > । ' p — , |l M , 111 pl 127 ,| ....................................... '' I ' ' ' ' I ' ' | । | | | | I ! ! I |”I I II | I I I I | 37.40 37.60 37.80 38.00 m/z 43.20 50.28% /z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #13489: 2-Propenoic acid, n-pentadecyl ester 55

5000 43 73 37.40 37.60 37.80 38.00 J 84 97 m/z 57.10 49.28%

n/z- > O—T , . , h ld 20 40 qh—l— • ' r -- m ' ' l"' ' 60 80 100 111 127 all— .1 139 153 166 182 120 140 160 180 200 210 । 1 ''' 1 i 1 ■ r 1 । 1 r ' ■ । 220 240 Abundance #111268: Dodecyl acrylate 55

37.40 37.60 37.80 38.00 5000 41 m/z 83.10 43.26% 73 1 0 ■ i ' 1 1 1 i 1 1 1 I 84 97 - 111 127 140 168 TTIT z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #13707: 5-Octadecene, (E)- .............. ... ................................... 55 37.40 37.60 37.80 38.00 m/ Z 69.10 42.20% 43 69 83 5000 97 29 111 — Il | 125 139 154 168 181 196 224 252 O-T4 , ’ ’ 1 i ■ ■ 1' i ' 1 ' ■ I ' ' r' i ' 1 ■ ■ i 1 1 1 1 I 1 1 1 1 I 1 1 1 1 I 1 1 ' 1 1 T"' 1 1 1 1 1 "iI I m/z—> 20I 40 60 80 100 120 140 160 180 200 220 240 37.40 37.60 37.80 38.00

NYC-WTC_000047399

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NYC-WTC_000047399Source: NYC Law Department, mirrored locally

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