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GCMS analysis results for sample AE08427, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE08427 conducted on May 6, 2002, including surrogate recovery data.

NYC-WTC_000048182–000048194

Folder label: “GCMS X 4/9/02 A 4/19/02”

←Page 12 of 13→
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020419\08427.D Vial: 14 Acq On 19 Apr 2002 8:56 pm Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 6 2-Fluoro-4-methyl-10H-acrid. .. Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

40.44 0.24 ug/1 482083 Chrysehe-dl2 39.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Fluoro-4-methyl-lOH-acridin-9-one 227 C14H10FNO 1000210-25-9 45 2 6-Nitro-2-methylpyrrolo[2,3-g]qu... 227 C12H9N3O2 1000071-35-1 43 3 1-Methoxybenzene, -4-(2-hydroxybe ... 227 C14H13NO2 1000221-93-3 7 4 5-Cyano-8-dimethylamino-6-methox... 227 C13H13N3O 1000213-20-5 7 Abundance Scan 6359 (40.442 min): 08427.D (-6347) (-) m/z 227.10 100.00% Z7

5000 40 113 i J l —i ( I pe I I I I I I

or -99 . .57 , 73 85 170 198 | 40.20 40.40 40.60 40.80 ' 1 ■ ■ ■ • । ■ • • > । । 1— । । ■ .' i । . . , > । "I m/ Z 40.10 41.98% n/z—> 40 60 80 100 120 140 160 180 200 220 Abundance #89104: 2-Fluoro-4-methyl-1 OH-acridin-9-one 2.7

5000 198 40.20 40.40 40.60 40.80 m/z 113.50 26.86% 151 170

n/z-> 13 t

40 .5760 67,77.89 9? 113120125 140 t 1/t.nd*/TTTTTCT111cT00r|—r 80 100 140 160 ,184 180 ,il 208 200 220 Abundance #89088: 6-Nitro-2-methylpyrrolo[2,3-g]quinoline Z!7 /.

40.20 40.40 40.60 40.80 5000 181 m/z 226.20 16.76% 43 57 69 83 154 I. 97 ........................ | 169 | 197 ’ 1 ' i —r —IP n/z-> 40 60 80 100 120 140 160 180 200 220 Abundance #89118:1-Methoxybenzene,-4-(2-hydroxybenzylideneamino) 2.7 40.20 40.40 40.60 40.80 212 m/z 228.10 14.85%

5000

77 94 39 51 64 w ■ 4 , Il ' l, I . — 1*)**/*/*T104114, EFTC128 — 139 154 167 183 196. i DTKOTBDd/T/d/-OL ■ * i ■ ■ 1 ■ i ■ ■ ' ' i ■ ' m/z-> 40 60 80 100 120 140 160 180 200 220 40.20 40.40 40.60 40.80

08427.D SCAN020418.M Thu May 02 15:34:27 2002 Page 8

NYC-WTC_000048193

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NYC-WTC_000048193Source: NYC Law Department, mirrored locally

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