GCMS Analysis Results, Sample AE08261, April 22, 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08261.D Vial: 18 Acq On : 17 Apr 2002 11:29 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 12 IH-Azonine, octahydro- Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

35.06 0.30 ug/L 391682 Perylene-dl2 34.79

Hit# of 3 Tentative ID MW MolForm CAS# Qual

1 IH-Azonine, octahydro- 127 C8H17N 005661-71-2 1 2 Fenoxon sulfoxide 278 C10H15O5PS 006552-13-2 1 3 Oleylamine 267 C18H37N 000112-90-3 1 Abundance Scan 5442 (35.054 min): 08261.D (-5441) (-) m/z 40.00 100.00% 40

5000 130 264 96 209 -p-r-r-r-pTT 57 281

m/z—> 01 20 40 1.. I 60 80 100 i111111 1 11'1 120 140 160 180 200 220 240 _L 260 280 34 80 m/z 130.00 35 00 35 20 35 40 31.76% Abundance #108185: 1H-Azonine, octahydro- 30 4 3 56

70 5000 127 34.80 35 00 35 20 35.40 84 96 m/z 264.10 29.82%

n/z—> 01 —I 15

20 A ill 40 V 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #13 Fenoxon sulfoxide 1) 109

34.80 35.00 35.20 35.40 5000 m/z 96.00 23.87% 79 263 39 51 63 | 93 127

n/z—> 0- AlLd 4 1 139 155 171 188 203215 231 247 ,TTTTTTTTTTTTTTTT ' * ' 14 '' 278

Abundance 20 40 60 80 100 120 140 160 180 200 220 240 260 280

3) #996: Oleylamine AAAAAAAMau 34 80 35 00 35 20 35 40 m/z 209.00 23.46%

5000

. 55 — 154 18 43 1 II 81 95 114 ,10 168 182 196 210 224 267 A l “44 AAA M I4 Tl/Z—> 0 —

20 s1ak,ah 40 purphLi* -"11 '• TTPIIIPTPTTT | 126 140 60 80 100 120 140 160 180 200 220 240 260 280 34.80 35.00 35.20 35.40

08261.D 041702SCAN.M Thu Apr 18 09:47:24 2002 Page 17

NYC-WTC_000048307