GCMS results for sample AE07766, Apr 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020415\07766.D Vial: 28 Acq On : 16 Apr 2002 8:51 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 14 5-(Ethoxycarbonylmethylene)... Concentration Rank 2

R. T. EstConc Area Relative to ISTD R.T.

31.15 0.43 ug/L 436417 Chrysene-dl2 30.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 5-(Ethoxycarbonylmethylene)cyclo ... 239 C13H21NO3 1000106-11-2 7 2 Azetidine, 1-methyl- 71 C4H9N 004923-79-9 7 3 3(2H)-Pyridazinone, 4,5-dihydro-... 112 C5H8N2O 005157-08-4 5 4 1-Azacyclononan-2-one 141 C8H15NO 000935-30-8 4 Abundance Scan 4777 (31 147 min):07766.D (-4771) (-) m/z 40.20 100.00% 43

5000

56 71 112 241 83 123 TII i ' ' 1 ' i 1 ■ ■ ■ i ■ ' 1 ■ I 1 ... ......................................... ...................... 30 80 31 00 31 20 31.40 olTl ■ i 1 ■ m/z 112.30 27.95% Tl/Z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #414: 5-(Ethoxycarbonylmethylene)cyclooctanone o-methyloxime 29 41

5000 AA........ 112 30 80 31 00 31 *20 31.40 U 55 79 93 126 m/z 109.30 25.24% 166 208

Olurii 1 L 194 239

n/z-> 20 40 60 80 I 100 I 120 | 140 II 160 180 I 200 1 220 240 Abundance 23

42 #119: Azetidine, 1-methyl- n/lnutenowwes 30 80 31.00 31.20 31 40 5000 m/z 71.30 24.92% 56

WW\puustu 71

—— Ol i ■ n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #46 3(2H)-Pyridazinone, 4,5-dihydro-6-methyl- 27 39 30 80 31 00 31 20 31 40 m/z 241.30 24.70% 112 5000- 55 83

0 IT I, , n/z-> 20 80 100 120 140 160 180 200 220 240 30 80 31 00 31.20 31.40

07766.D 041202SCAN.M Tue Apr 16 13:42:17 2002 Page 17

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