Laboratory report documenting GCMS analysis of sample AE08425 conducted on May 6, 2002, including surrogate recovery data.
NYC-WTC_000048148–000048168Folder label: “GCMS X 4/9/02 A 4/19/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\MSDCHEM\1\DATA\020419\08425.D Vial: 12 Acq On : 19 Apr 2002 6:58 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e
Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1
Peak Number 7 Azetidine, 1-methyl- Concentration Rank 14
R.T. EstConc Area Relative to ISTD R.T. 36.42 0.22 ug/1 387203 Chrysene-dl2 39.93 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Azetidine, 1-methyl- 71 C4H9N 004923-79-9 7 2 Cyclobutanone, 2-methyl-2-oxiranyl- 126 C7H10O2 075314-19-1 6 3 2-Methyl-pyrroline 83 C5H9N 1000143-24-0 5 4 2-Ethoxy-2-cyclohexen-l-one 140 C8H1202 029941-82-0 5 Abundance Scan 5675 (36.423 min): 08425.D (-5667) (-) m/z 40.10 100.00% 43
5000 55 83 69 97 111 125
n/z-> 20 1 —49,50 1 60 ■ i ' ■ 1 ' i ' ‘ 30 40 ' i ■ ■ 70 .. I..... 80 90 100 I 110 120 I - 140 130 140 36.00 36.20 36.40 36.60 36.80 m/z 55.05 44.11% Abundance
bu #119: Azetidine, 1-methyl- 23
42 5000 56 36.00 36.20 36.40 36.60 36.80 71 m/z 83.00 40.84%
m/z-> 1 ।1 ' 20 Il. l——7, 30 40 50 [ rr r1 । i ' 1 60 70 80 90 100 110 120 130 140 Abundance #1251: Cyclobutanone, 2-methyl-2-oxiranyl- 39 55 69 mun nqlwv " 36.00 36.20 36.40 36.60 36.80 m/ z 57.10 39.95%
wlww 5000 83 98 —— ' i 1 ■ TT ■ ।'1 ■11 ■ ■ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #1092: 2-Methyl-pyrroline 31 36.00 36.20 36.40 36.60 36.80 m/ Z 43.20 39.42%
n/z-> 5000
20 30 40 43 50 55 | 60 68 70 80 83 90 100 110 120 130 140 AVAa. Pr ' 1 o ... P. I I I I I I I 1 I I I 1 36.00 36.20 36.40 36.60 36.80
08425.D SCAN020418.M Thu May 02 15:28:11 2002 Page 9
NYC-WTC_000048160
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NYC-WTC_000046864
Laboratory report documenting GCMS analysis of sample AE07766 including surrogate recovery and unknown compounds on April 18, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048121
Laboratory report documenting GCMS analysis of sample AE08431 conducted on May 6, 2002, including surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048355
GCMS analysis report for sample AE08264 showing surrogate recovery and unknown compound screening on April 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048106
Laboratory report documenting GCMS analysis of sample AE08323 conducted on May 6, 2002, including surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048134
Laboratory report documenting GCMS analysis of sample AE08324 conducted on May 6, 2002, including surrogate recovery data.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047926
GCMS analysis report for sample AE08258 showing surrogate recovery and unknown compounds from April 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048287
Initial analysis page for sample AE08261 showing surrogate recovery data and unknown compound screening.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048401
GCMS analysis report for sample AE08266 showing surrogate recovery and unknown compound screening on April 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048378
GCMS analysis report for sample AE08265 showing surrogate recovery and unknown compound screening on April 22, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047886
GCMS analysis report for sample AE08256 showing surrogate recovery and unknown compounds from April 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047802
Laboratory report documenting GCMS analysis of sample AE08252 conducted on April 19, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048309
GCMS analysis report for sample AE08262 showing surrogate recovery and unknown compound screening on April 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000048081
Department of Environmental Protection GCMS analysis record dated April 9-19, 2002.
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NYC-WTC_000048082
Fragmented document page containing metadata and identifiers related to GCMS testing procedures from early April 2002.
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NYC-WTC_000048085
Laboratory report showing non-detect results for volatile organic compounds in a GCMS blank run (Sample AE08323) from April to May 2002.
Filed in the same folder
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Laboratory report of GCMS calibration (Sample AE08323) conducted between April 9 and May 3, 2002, showing response factors for volatile organics.
Filed in the same folder
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Laboratory report of GCMS reference standard run (Sample AE08323) conducted between April 9 and May 3, 2002, verifying instrument performance.
Filed in the same folder