GCMS analysis results for sample AE07772, April 18, 2002

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Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020404\07772 . D Vial: 26 Acq On 5 Apr 2002 6:13 am Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title Method 508 GC/MS Scan Library C:\DATABASE\nist98.1

Peak Number 2 Cyclopropanecarboxylic acid Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 3.31 0.31 ug/1 230637 1,4-Dichlorobenzene-d4 10.66

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopropanecarboxylic acid 86 C4H602 001759-53-1 3 2 Azetidine, 1-nitroso- 86 C3H6N20 015216-10-1 2 3 3-Butenoic acid 86 C4H602 000625-38-7 2 4 1,4-Dioxin, 2,3-dihydro-_____________ 86 C4H602 000543-75-9 1 Abundance Scan 40 (3.314 min): 07772. D (-33) (-) m/z 40.10 100.00% 40

5000

1111"1‘E0E0011011111"‘CCDTTTTOIT 47 86 3.20 3.30 3.40 3.50 3.60 3.70 ----- Oh m/z 86.00 13.10%

w/"MMMwhwod ■ i ■''11 ■' " i1''' r 1 m/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1243: Cyclopropanecarboxylic acid 39

5000 42 85 45 58 3.20 3 30 3.40 3.50 3.60 3.70 27 68 m/z 47.00 12.63% 55 Or ’' i ■ —25ll30H 3 40 145 5050 1 M55111 60' l'1 ■ 65 70 75 80 85 90 95 31 TPTTTTT 71 1 ■ ‘11 ■1111 ‘ MWWMs h m/z-> 15 20 35 Abundance #734: Azetidine, 1 -nitroso- 33 111'' ■ ■ i ■11 r1 11 - TT 3.20 3.30 3.40 3.50 3.60 3.70 41 5000 86 44 55

. 52 , 69 O- ′′′′′′′′′ H 1 3£ +...... 1111 I tn I i I I I | I I I I | t r 177 I 1' ।'1'' । 1 ITTn I' m/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1245: 3-Butenoic acid 33

5000 12 45 58 86 29 20 i Oh .... ........ llil, TIT 55 1111 63 68 72 111111111111 ft । ■ i ■1 ■ ■ । ■ ' H '1 r ' 1 1 i' m/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95

07772 .D SCAN020403 .M Wed Apr 10 11:30:40 2002 Page 4

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