GCMS results sample AE08254, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020417\08254.D Vial : 12 Acq On : 17 Apr 2002 6:32 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 6 Pyrazine, methoxy-, 4-oxide Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 35.07 0.22 ug/L 286674 Perylene-dl2 34.79 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Pyrazine, methoxy-, 4-oxide 126 C5H6N2O2 023902-69-4 2 2 IH-Azonine, octahydro- 127 C8H17N 005661-71-2 1 3 IH-Azonine, octahydro- 127 C8H17N 005661-71-2 1 4 Oleylamine 267 C18H37N 000112-90-3 1 Abundance Scan 5445 (35 072 min): 08254.D (-5443) (-) m/z 40.00 100.00% 43

5000

96 118 208 34 80 35 00 35 20 35.40 0- I 130 265 TTIUPPTTTpT i ' ' 1 ' i 1 ■' 1 i 1 1 ' 1 i ■ 1 ' 1 i ' 1 1 ■ i ' m/ z 36.00 21.37% n/z--> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #1411: Pyrazine, methoxy-, 4-oxide 4b

52 5000- 96 126 m/Z 117.90 18.80%

n/z-> 0- 20 40 I .4 % . 60 80 100 110 120 140 160 180 200 220 240 260 Abundance #108185: 1H-Azonine. octahydro- 30 43 56

70 34.80 35.00 35 20 35 40 5000- m/z96.10 17.84% 127 84 96 15 I Ll.1 m112al । 0^ ■ ■ i 'i । ' ■ - Tl/Z-> Abundance 20 40

30 43 _ 56 60 80 100 120 140 #744: 1H-Azonine, octahydro- 160 180 200 220 240 260 LAAAALAAAAAAAAd 34 80 35 00 35 20 35 40 m/z 208.00 17 .37% 70 5000 127 84 98

■n/z-> 0- 15 20 40 — —L l ■ a I d ' 60 80 100 112

120 140 160 180 200 220 240 260 34 8 0 35.00 35.20 3 5 40

08254.D 041702SCAN.M Thu Apr 18 09:23:31 2002 Page 11

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