GCMS analysis report, sample AE07568, April 2002

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Data File C:\MSDCHEM\l\DATA\020403\07568.D Vial: 16 Acq On 3 Apr 2002 10:56 pm Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 6 2-Amino-2-oxo-acetic acid, . Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T.

43.01 0.50 ug/1 369332 Perylene-dl2 42.30

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Amino-2-oxo-acetic acid, N-[3,... 221 C12H15NO3 1000127-85-3 5 2 Furo[2,3-c]pyridine, 2,7-dimethyl- 147 C9H9NO 069022-77-1 4 3 Cyclopropanamine, N-methyl-l-phe... 147 C10H13N 056771-48-3 4 4 2-Indolizinemethanol 147 C9H9NO 022320-21-4 4 Abundance Scan 6796 (43.010 min): 07568. D (-6787) (-) m/ z 73.10 100.00% 73 147 221 5000 281 355 ............... I l.ir........ 42.60 42.80 43.00 43.20 43.40 40 Aso 1 1 PPr a 0+ Thn) 1111 11111111 m/ Z 147.10 75.10% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #87891: 2-Amino-2-oxo-acetic acid, N-[3,4-dimethylphenyl]-... 221 1 _

5000 120 147 —....... 11c..,. 42.60 42.80 43.00 43.20 43.40 m/z 221.10 55.01% 77 105 m/z-> oW 40 514444 1165 193 60 r11111Ti 11111 11 ■ ■ ■ i ' i' ' 1 I ' ' 1 ' I ‘ 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ' I 111111111' I ■'1' 1

Abundance #65810: Furo[2,3-c]pyridine, 2,7-dimethyl- yyAM 147 i ■ ' i ■ ' 42.60 42.80 43.00 43.20 43.40 5000 m/z 207.00 34.72%

m/z- > 01 „I l 51 ... 778.... ,b i ■n■i1■■ ■ i ■ ■ ■' i ■ I..... 118

40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 1' ■ ■ ■ 1 ■ ■ ■11

Abundance #65785: Cyclopropanamine, N-methyl-1-phenyl- 147 42.60 42.80 43.00 43.20 43.40 m/z 281.00 31.77% 5000

43 j — 132

| 77 105 I l 0 I — "eu/*14fh1 I Hi " 14| ! it, | 4, I | I ! I । ■ ■ ■ ■ । ■ 1 ■ ■ ■ • । ■ ■ ■ ■ । ■ 11111111' 1111 ■111 >' 11 ■ m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 42.60 42.80 43.00 43.20 43.40

07568.D SCAN020403.M Thu Apr 04 10:30:38 2002 Page 8

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