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← Document results/DEP Box 27/GCMS X 4/2/02 A 4/3/02
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GCMS analysis report, sample AE07568, April 2002

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Laboratory results for unknown compounds and surrogate recovery in sample AE07568 analyzed on April 9, 2002.

NYC-WTC_000047195–000047215

Folder label: “GCMS X 4/2/02 A 4/3/02”

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Data File C:\MSDCHEM\l\DATA\020403\07568.D Vial: 16 Acq On 3 Apr 2002 10:56 pm Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 7 1H-1,2,4-Triazole, 3,5-diph... Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T. 43.27 0.19 ug/1 137446 Perylene-dl2 42.30 Hit# of 5 Tentative ID MW MolForm CAS# Qual l 1H-1,2,4-Triazole, 3,5-diphenyl- 221 C14H11N3 002039-06-7 2 2 (E)-2-Hydroxy-4'-cyano-stilbene 221 C15H11NO 1000147-85-5 2 3 6-Phenyl-3,5-dithioxo-2,3,4,5-te... 221 C9H7N3S2 1000147-85-6 2 4 Furfurylideniminosulphur pentafl... 221 C5H4F5NOS 090598-15-5 1 Abundance Scan 6840 (43.268 min): 07568.D (-6828) (-) m/z 221.00 100.00% 221

5000 40 73 147

207 / i* 43.00 43.20 43.40 43.60 0 " i" " I" " i" " r'" P111 r "1P "1P " ‘ I"11P1" P1" P 1111" ITT 1" Irrri P111P11 ‘T’’ 111 m/z 147.10 32.14% m/z—> 30 40 50 60 70 80 90 100110120130 140150 160 170180 190 200 210 220 Abundance #126939:1H-1,2,4-Triazole, 3,5-diphenyl- 1 8 221 [ I AMAA

5000 91 ...7. 43.00 43.20 43.40 43.60 63 77 m/z 40.10 31.55% 39 51 .... I..... I 0 r ’" i" " i1 I... ... 1....... 'i" " ।।" p11! ।" 111 193 11"1 r " ■ I" " r1" i" " r " ■ r ■" r "' r " ■ r ■" r " ■ i m/z-> 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 220 Abundance #87938: (E)-2-Hydroxy-4'-cyano-stilbene Z!1

43.00 43.20 43.40 43.60 5000 m/z 73.10 22.02%

165 190 — 152 । 177 । 206 0 i'1" i " " r r 1 r i" " p " ■ r " 11 ................................................i........... lii........ h r 1" i" " i" " i'1" i" " 11"1111,111111111 HH ‘ ‘‘i nfe-> 30 40 50 60 70 80 90 100110120130140150160170180190200 210 220 Abundance #87936: 6-Phenyl-3,5-dithioxo-2,3,4,5-tetrhydro-1,2,4-triazin . । । ANY,, . 22 !1 43.00 43.20 43.40 43.60 m/z 207.00 12.02% 77 89 104 5000 118 60 51 133 42 162 .... — 0 "‘‘i TTTTT T’T r1111 | | | 1 • । | H | H I i | i H . | . T’TI n/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 220 43.00 43.20 43.40 43.60

07568.D SCAN020403.M Thu Apr 04 10:30:39 2002 Page 9

NYC-WTC_000047207

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