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GCMS analysis report, sample AE07568, April 2002

Machine-extracted title · confidence 100%

Laboratory results for unknown compounds and surrogate recovery in sample AE07568 analyzed on April 9, 2002.

NYC-WTC_000047195–000047215

Folder label: “GCMS X 4/2/02 A 4/3/02”

←Page 14 of 21→
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\020403\07568.D Vial 16 Acq On 3 Apr 2002 10:56 pm Operator Nefliu Sample sample Inst Instrumen Mise Multiplr 1.00 MS Integration Params: LSCINT.e

Quant Method : C: \MSDCHEM\1\METHODS\SCAN020403 .M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 8 Adenosine, 2-methyl- Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

43.29 0.15 ug/1 112683 Perylene-dl2 42.30

Hit# Of 4 Tentative ID MW MolForm CAS# Qual

l Adenosine, 2-methyl- 281 C11H15N5O4 016526-56-0 1 2 Acetic acid, 4-(3-acetylamino-2-... 249 C13H15NO4 1000194-74-7 1 3 Diethyl 3-chloro-2-hydroxypropyl... 252 C10H17C1O5 1000222-74-8 1 4 2-Methoxy-5H-indolo[2,3-b]quinox... 249 C15H11N3O 1000223-36-6 1 Abundance Scan 6844 (43.292 min): 07568.D (-6841) (-) m/z 40.10 100.00% 43

5000 281

207 43.00 43.20 43.40 43.60 ..................... 1......... 1 01 i r ' ■ i ■1111''' ■ ।'1' ■ । ■111111'' । ■ ■' ■ ।1''' । '1 ■ ।1''' ।111111 ■r 11111' ।11 m/z 2 81.00 49.23% n/z-> :20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #1079: Adenosine, 2-methyl- 31

— 5000 45 43.00 43.20 43.40 43.60 59 74

7 149 178 m/z 207.00 10.91% , 4 „ , 86 108120133 | 163 | 192 206 239251264 281 0 I 1 1 TTTtr 'll!'1 . 1 , i r । । । n , ( r\ , T ! I I'l 1-1 T I | I I | I -| I!"i -r |-r I ! | |' I , m/z-> :20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #933: Acetic acid, 4-(3-acetylamino-2-oxopropyl)phenyl ester 33 107

43 43.00 43.20 43.40 43.60 5000 72

120 207 249

0 TH --4— 1191.44..- TTurr 57 134 149 165177189 1.. 230 | . . , ' I' ' ■ 1 i ■ ■ ■ ■ i ■

m/z-> :20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #642: Diethyl 3-chloro-2-hydroxypropylmalonate 29 207 43 115

5000 137 75 87 165 57

m/z-> ___L 1191.a L 0 i ' r 1 1 i ' 1 1 ' [1 ' * 1 । • 20 40 60 80 । I TTPTIPPPD 187 ' 1 I ' ' ' ' I ' ' ' ' I ' ' 100 120 140 160 180 200 220 240 260 280

07568.D SCAN020403 .M Thu Apr 04 10:30:39 2002 Page 10

NYC-WTC_000047208

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NYC-WTC_000047208Source: NYC Law Department, mirrored locally

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