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GCMS analysis report, sample AE07520, April 2002

Machine-extracted title · confidence 100%

Laboratory results for volatile organic compounds in a GCMS blank sample analyzed on April 2-3, 2002.

NYC-WTC_000047159–000047176

Folder label: “GCMS X 4/2/02 A 4/3/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\020403\0402LB.D Vial: 10 Acq On 3 Apr 2002 5:21 pm Operator: Nefliu Sample 04/02 lab blk Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title Method 508 GC/MS Scan Library C:\DATABASE\nist98.1 Peak Number 11 Adenosine, 2-methyl- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

44.78 0.29 ug/1 213432 Perylene-dl2 42.30 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Adenosine, 2-methyl- 281 C11H15N5O4 016526-56-0 3 2 Pyrido[2,3-d]pyrimidin-4(1H)-one 147 C7H5N3O 024410-19-3 2 3 1H-Imidazo[4,5-b]pyridine-2-carb... 147 C7H5N3O 056805-24-4 2 4 1-Naphthalenamine, 5,6,7,8-tetra... 147 C10H13N 002217-41-6 2 Abundance Scan 7097 (44.778 min): 0402LB.D (-7088) (-) m/z 73.10 100.00% 73 147 221 207 5000 281 40 44.40 44.60 44.80 45.00 45.20 oh m/z 147.10 75.50% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #1079: Adenosine, 2-methyl- 31

5000 45 ■ I • ‘7T‘I 1 T-r 44.40 44.60 44.80 45.00 45.20 59 74 m/z 221.00 61.46% 149 178 , d. . , .86 86 108120 133 J 163 | 192 206 239251264 281 Oh i ....... "-ri Tr‘T' |- r 1 11 । । । r । । । "i । । ।'■(■"i i 1‘T"I । I N‘‘IIrrJ ।—rTrp । ■ । ■'! i J । । । । j11 । m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #66005: Pyrido[2,3-d]pyrimidin-4(1 H)-one 147 44.40 44.60 44.80 45.00 45.20 5000 m/z 2 07.00 51.50%

nri/z- > Abundance 0 20 38 50 64 76 92 119

- doih,j JI - ' I 1 ' ' 1 1 / pr I I I | I I ! I |, 40 60 80 100 120 140 160 180 200 220 240 260 280 #66006:1 H-lmidazo[4,5-b]pyridine-2-carboxaldehyde A J 92 14,7 44.40 44.60 44.80 45.00 45.20 m/z 281.00 32.65% 119 5000 A 65

op T-rj-T-T-TT-p-rTT-p-T 1 1 1 ■ ' ■ 1 1 1 1 1 i ■ ,-l 1 1 ti 1 ' I ' r ’ ‘I I ' I I I I m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 44.40 44.60 44.80 45.00 45.20

0402LB.D SCAN020403 .M Thu Apr 04 10:14:27 2002 Page 13

NYC-WTC_000047174

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NYC-WTC_000047174Source: NYC Law Department, mirrored locally

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