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← Document results/DEP Box 27/GCMS X 4/2/02 A 4/3/02
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GCMS analysis report, sample AE07568, April 2002

Machine-extracted title · confidence 100%

Laboratory results for unknown compounds and surrogate recovery in sample AE07568 analyzed on April 9, 2002.

NYC-WTC_000047195–000047215

Folder label: “GCMS X 4/2/02 A 4/3/02”

←Page 18 of 21→
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Data File C:\MSDCHEM\l\DATA\020403\07568.D Vial: 16 Acq On 3 Apr 2002 10:56 pm Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 12 2-1-Phenyl ethylidene-hydra... Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T. 43.53 0.11 ug/1 79954 Perylene-dl2 42.30 Hit# of 2 Tentative ID MW MolForm CAS# Qual 1 2-1-Phenyl ethylidene-hydrazono-... 281 C16H15N3S 1000148-55-3 3 2 Adenosine, 2-methyl- 281 C11H15N5O4 016526-56-0 1

Abundance Scan 6885 (43.533 min): 07568.D (-6881) (-) m/z 40.10 100.00% 43

8000 281 6000

4000 43.20 43.40 43.60 43.80 m/Z 2 81.00 64.08% 2000 73 0|.■ । । । 1 207 221 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #97319: 2-1-Phenyl ethylidene-hydrazono-3-methyl-2,3-dihyd... 281 TTT 43.20 43.40 43.60 43.80 8000 m/Z 73.10 6.57% 6000

4000 150 77 163 109 136 2000 91 43.20 43.40 43.60 43.80 65 || 223 252 266 n/z-> 20 oh ............ Ill 40 60 80 100 441,22. M,"........... 7.....11. 120 140 160 180 200 220 240 260 280 m/z 221.10 0.70%

Abundance #1079: Adenosine, 2-methyl- 31 8000

6000 - X/ . । | . ... | ■ > ! I | -- 43.20 43.40 43.60 43.80 TTT

45 m/z 207.00 0.12% 4000 ./ 59 74 2000 I 149 178 m/z-> ob 20 ,) Ji,40#.60+ 272485. 198129133, . 1163,1 .... ,.?81, 80 100 120 140 160 180 200 220 240 260 280 43.20 43.40 43.60 43.80

07568.D SCAN020403.M Thu Apr 04 10:30:39 2002 Page 14

NYC-WTC_000047212

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NYC-WTC_000047212Source: NYC Law Department, mirrored locally

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