GCMS analysis results for sample AE11382, May 22 2002

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Laboratory report showing GCMS analysis results for sample AE11382 conducted on May 22, 2002.

NYC-WTC_000025127–000025144

Folder label: “GCMS X 5/15/02 A 5/17/02”

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NYC 9/11 Public Portal Document Llprary search compound Report Data File : C:\MSDCHEM\1\DATA\051702\11381.D Vial : 8 Acq On : 17 May 2002 6:29 pm Operator: Mclean Sample : 5/15 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L * • ******************************************************************* Peak Number 4 Anthracene, 2-methyl- Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T. 22.58 0.31 ug/L 412092 Phenanthranene-dl0 22.95 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene, 2-methyl- 192 C15H12 000613-12-7 64 ' 2 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5 50 3 2,5-Dihydrophosphole, 3-methyl-1... 192 C11H13OP 1000196-97-5 45 4 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 42 Abundance Scan 3319 (22.580 min): 11381 .D (-3310) (-) m/z 192.10 100.00% 192

5000

42 52 70 82 96 146 160 22.20 22.40 22.60 22.80 23.00 0 1111 < 1111111111 M1‘ 11111 il 11 i'i 1111I1111 118 ' r " 1 r '11 r 1 -H - m/z 191.10 21.52% m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125847: Anthracene, 2-methyl- 192

5000 — 22.20 22.40 22.60 22.80 23.00 m/ Z 146.00 15.23% 28 39 51 63 82 96 115 126 139 152 165 176 0 1j>> । ■11‘| 111 > I'1 ■.. । i'i । ■ j. rri i'i1, I’ll 11'1‘f 11111 p-ri 11111111111'| 1111 |'i 11111T11111 I'i 111'I'l TIum mlz-> 20 30 40 50 60 70 80 90 100 110 120 130.140 150 160 170 180 190 200 Abundance #80950:1,5-Naphthalenedithiole 192 ......A.... .. 22.20 22.40 22.60 22.80 23.00 5000 m/z 96.00 14.12% 115 128 159 40 57 69 79 96 147

miz-> Of -------------- L 177 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 -n-rpnrrh-p-TT ■n-p-r

Abundance #80965: 2,5-Dihydrophosphole, 3-methyl-1 -oxo-1 -phenyl- .......... , 192 22.20 22.40 22.60 22.80 23.00 164 m/z 193.00 14.12% 5000 99 115 47 77 177 67 125 134 146 m/z-> 0 —2738.57 mt4+ 1ll++++155— HH rt , । 871 II I 1' r 1 i i > ■ ■ । । ■ * 1 । 1 * * 1 । 1 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80 23.00

11381.D 050102.M Tue May 21 14:25:29 2002 Page 7

NYC-WTC_000025138

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GCMS analysis results for sample AE11381, May 22 2002 · Box DEP Box 18

NYC-WTC_000025102

Laboratory report showing GCMS analysis results for sample AE11381 conducted on May 22, 2002.

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