GCMS analysis results for sample AE11382, May 22 2002

NYC 9/11 Public Portal Document uiprary bearcn compound KepOIC

Data File : C:\MSDCHEM\l\DATA\051702\11381.D Vial: 8 Acq On : 17 May 2002 6:29 pm Operator: Mclean Sample : 5/15 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 5 Anthracene-dlO- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.45 ug/L 596776 Phenanthranene-dl0 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual

I Anthracene-dlO- 188 C14D10 001719-06-8 90 2 Phenanthrene-diO 188 C14D10 001517-22-2 86— 3 2,2,9,9-Tetramethyldec-5-ene-3 ,7... 188 C14H20 102745-35-7 38 4 Pentacyclo[7.3.1.1. (4,12) .0 (2,7) . .. 188 C14H20 1000215-61-8 38 Abundance Scan 3409 (23.109 min): 11381 .D (-3402) (-) m/z 188.10 100.00% 188

5000 - 80 94 22.80 23.00 23.20 23.40 0 ....................... .. 1 ' | 43 | 54 66 I । 1 l‘. P । । 1 | 1 ■ I i | I I I I | I I I 132 mTTT 158 i11" i m/Z 189.10 17.96% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

........ ) 5000 T’II’IIII 22.80 23.00 23.20 23.40 m/z 184.10 16.95% 80 94 160 . I 17 30 42 52 66 IT146—4179179— ‘1 108 118 132 0 TI— nu — mnu-tmHhr I rt It I ■! rl I Iit miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188

22.80 23.00 23.20 23.40 5000 m/z 94.10 14.18%

80 94 160 30 42 52 66 1 108118 132 146—4170179 — 0 TTTTTTTTTTTTTTTTTTTHTTTHTTH I I rT71 ri r । i Ti i [ i ! । i [ 111 11 i m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79801:2,2,9,9-Tetramethyldec-5-ene-3,7-diyne ..................................................... 188 22.80 23.00 23.20 23.40 173 m/z 80.05 12.79% 41 131 143 91 A 5000 77 158 57 119 27 67 105

m/z-> 0 — 1 p-rrt | + 14 + 1444 114 4—444—4 MI U 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

11381.D 050102.M Tue May 21 14:25:31 2002 Page 8

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