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GCMS blank analysis results for sample AE11410, May 22 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS blank analysis for sample AE11410 conducted on May 22, 2002.

NYC-WTC_000025216–000025233

Folder label: “GCMS X 5/15/02 A 5/18/02

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Scanned page image, NYC-WTC_000025226
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NYC 9/11 Public Portal Document Llbrary bearen compound Keport

Data File : C:\MSDCHEM\1\DATA\051702\0515LB.D Vial: 16 Acq On : 18 May 2002 1:49 am Operator: Mclean Sample : 5/15 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 4 Anthracene-d10- Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T.

23.11 0.34 ug/L 493930 Phenanthranene - dl 0 22.95 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dl0- 188 C14D10 001719-06-8 91V 2 Phenanthrene-diO 188 C14D10 001517-22-2 91/7 3 1,4-Naphthoquinone, 2,3-dihydro-... 188 C12H12O2 1000157-22-3 40 4 2,2,9,9-Tetramethyldec-5-ene-3,7... 188 C14H20 102745-35-7 38 Abundance Scan 3409 (23.109 min): 0515LB.D (-3403) (-) m/z 188.10 100.00% 188

5000

42 52 64 80 94 132 160 22.80 23.00 23.20 23.40 O-P TTHTmPPmmmmpT 1 207 TTTTTTTTTTTT m/ z 189.15 16.05% m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #79826: Anthracene-d10- 188

5000 ------- 22.80 23.00 23.20 23.40 m/z 184.10 15.03% 80 94 160 17 30 42 52 66 108118 132 146 1 170 0 I" " I" " I" " 11"11111 ■ 1111. J"11 11" " I'" mfe-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #79827: Phenanthrene-d10 188 ..................................................... 22.80 23.00 23.20 23.40 5000 m/z 94.10 10.33%

80 94 160 30 42 52 66 , 108118 132 146 .|| 170 I 0 I'" 'I.... . .......... . . 1111u ।.111111H11n11 11 ■"' i"1 m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #79805:1,4-Naphthoquinone, 2,3-dihydro-5,8-dimethyl- ... 188 22.80 23.00 23.20 23.40 173 m/z 80.10 10.17% 5000 145 82 91 159 65 , 115। . 131 27 39 51 105

m/z-> 0 i■ r11 TTTTT pillrsy# ras +44+ T+ Ar 11 r J' 11 r lm p i ----- 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 22.80 23.00 23.20 23.40

0515LB.D 050102.M Tue May 21 16:00:09 2002 Page 7

NYC-WTC_000025226

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NYC-WTC_000025226Source: NYC Law Department, mirrored locally

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