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GCMS analysis results, sample AE12324, June 2002

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Gas chromatography mass spectrometry results for sample AE12324 including surrogate recovery data analyzed on June 7, 2002.

NYC-WTC_000014303–000014329

Folder label: “GCMS X 5/24/02 A 5/29/02

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NYC 9/11 Public Portal Document Library searen Compound Report

Data File : C:\MSDCHEM\1\DATA\052902\12324.D Vial: 12 $ Acq On : 29 May 2002 7:03 pm Operator: McLean Sample : gc/ms scan 5/24 fb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : G:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 18 Anthracene-dlO- Concentration Rank 15

R.T. EstConc Area Relative to ISTD R.T. 23.06 0.32 ug/L 328987 Phenanthranene- dl 0 22.91

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-dlO- 001719-06-8 72 188 C14D10 2 Phenanthrene-diO 001517-22-2 64— 188 C14D10 3 Benzene, 1-(1-cyclohexen-l-yl)-4... 188 C13H160 020758-60-5 42 4 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 40 Abundance Scan 3401 (23.062 min): 12324.D (-3395) (-) m/z 188.10 100.00% 188

5000

94 80 160 22.80 23.00 23.20 23.40 43 52 66 0-TIWWNIPPTLTTTTTNT -H m/z 94.00 18.19% n/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180 190 Abundance #79826: Anthracene-d10- 188

5000 22.80 23.00 23.20 23.40 m/z 189.10 16.29% . 80 94 160 17 30 42 52 66 . | 108118 132 146 0 DmmTTTH ii 11| 11 ■ 1111111 ii 1111111 [ 11 rr| fr ..I,I. 170179 n/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188 Baag 22.80 23.00 23.20 23.40 5000' m/z 184.10 15.57%

80 94 160 30 42 52 66 11 108118 132 146 tI, 170179.,I 0 mmpmpHpH I I . I | ■ ! 11 , . I , I | . ! . . | I ■ . . | I . |7| . r’tr I I l'| I 11 ITtt .. >. n/z-> 10 2030405060 70 8090 100110120 130140150160170180190 Abundance #79791: Benzene, 1 -(1 -cyclohexen-1 -yl)-4-methoxy- 188 22.80 23.00 23.20 23.40 m/z 80.10 11.63%

5000 160

115 129 145 173

/z-> 41 51 65 0 ------------- |Z | 102 77 4444144+47el 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 4 mm 22.80 23.00 23.20 23.40

12324.D 052202.M Mon Jun 03 10:52:29 2002 Page 21

NYC-WTC_000014328

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NYC-WTC_000014328Source: NYC Law Department, mirrored locally

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