GCMS analysis results for sample AD31643, Jan 28 2002

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Data File : C:\MSDCHEM\1\5973N\02JAN17\31643.D Vial: 3 • Acq On : 17 Jan 2002 4:29 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 17, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 Anthracene-D10 Concentration Rank 2

R.-T. EstConc Area Relative to ISTD R.T. 22.77 0.35 ug/L 203644 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-D10 188 C14D10 000000-00-0 91 2 Phenanthrene-diO 188 C14D10 001517-22-2 86 3 Anthracene-dlO- 188 C14D10 001719-06-8 74 4 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 56 Abundance Scan 1699 (22.771 min): 31643.D (-) m/z 188.15 100.00% 188

5000

94 i । i . । i i P r i i i । i i । i । i 52 66 80 160 22.40 22.60 22.80 23.00 23.20

n/z-> 40 O' 11 ■■ r ■1 30 40 50 60 70 80 m*PPP 90 1W 110 120 130 140 150 160 170 180 190 M. m/z 94.10 18.15% Abundance #84498: Anthracene-D10 14®

.. „ i i । , i । [ i 5000 _____ / • i • ’ * • i • 22.40 22.60 22.80 23.00 23.20 80 m/z 189.10 16.82% 94 66 160 —

niz-> 0- ■111 ■" । 30 40 50 ।’1‘। “ p TTT 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84499: Phenanthrene-d10 188 00/ 22.40 22.60 22.80 23.00 23.20 5000 m/z 184.10 14.61%

80 94 160 p — —1— 66 0i mmpe nfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84502: Anthracene-d10- ________ j P"r r i । । i । i i । i ■ i 1 ■ ' 1 i ■ 1(18 22.40 22.60 22.80 23.00 23.20 m/z 80.05 12.50%

5000

0 mohjos l t I I I 1 1 I I I 66 Ji m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ______ / — ................. .. • । ■ ■ • ■ । ■ p1 '11111111 rT 22.40 22.60 22.80 23.00 23.20

31643.D SCAN508.M Tue Jan 22 08:37:14 2002 Page 10

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