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GCMS results for sample AE00700, Feb 13 2002

Machine-extracted title · confidence 100%

GCMS analysis log for sample AE00700 showing surrogate recovery and unknown compounds detected on February 13, 2002.

NYC-WTC_000051806–000051824

Folder label: “GCMS X 1/10/02 A 1/16/02

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Scanned page image, NYC-WTC_000051823
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document LlDrary searen compound Keport

Data File : C:\MSDCHEM\1\5973N\02FEB01\00700.D Vial: 7 - Acq On : 1 Feb 2002 7:42 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 Anthracene-d10- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

22.77 0.42 ug/L 286994 Phenanthrene-dl0 22.63

Hit# of / 5 Tentative ID MW MolForm CAS# Qual

1 Ant: acene-dlO- 188 C14D10 001719-06-8 80 2 DEC EUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 72 3 Acridine-D9 188 C13D9N 000000-00-0 64 4 Pnenanthrene-dlO 188 C14D10 001517-22-2 56 Abundance Scan 1699 (22.771 min): 00700.D (-) m/z 188.20 100.00% 188

5000

80 TI T T T bit 2 132 . 146 158 22.40 22.60 22.80 23.00 23.20 n/z-> 49 0 I ' ‘ * I' ' ' ' I 66 - । i' ■ ■ ■ i' 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 TBT L m/z 184.10 h 24.34% Abundance #84502: Anthracene-d 10- 118

5000 TT i ' 1 1 TT 22.40 22.60 22.80 23.00 23.20 m/z 189.10 17.71%

0 ।। 66 8 34 11 ■ ■ I ■ । ■11 > | ■1111111 > । I'''' I •''' I 160 ........ ill....... /z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188 ■ i ■ ■ ■ ■ i vr 22.40 22.60 22.80 23.00 23.20 5000 m/z80.05 16.01%

80 94

n/z-> 0T 66 11muummPTT 11" " 111111 " 1 i"1H " n ।' 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 158 .. 1.. Abundance #85254: Acridine-D9 188 22.40 22.60 22.80 23.00 23.20 m/ z 92.10 13.77% A 5000

0 ............................. ...... ......... l .. ------------------------------- m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 22.80 23.00 23.20

>0700.D SCAN508.M Mon Feb 04 08:40:52 2002 Page 14

NYC-WTC_000051823

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NYC-WTC_000051823Source: NYC Law Department, mirrored locally

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