GC/MS data fragment, May 28 2002

Machine-extracted title · confidence 90%

Fragmented document containing GC/MS data from May 28, 2002.

NYC-WTC_000025332–000025343

Folder label: “GCMS X 5/15/02 A 5/18/02”

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NYC 9/11 Public Portal Document ui.jji.axy oedicu COIpOUIC Kepox L Data File : C:\MSDCHEM\1\DATA\051702\11416.D Vial: 25 Acq On : 18 May 2002 9:10 am Operator: Melean Sample : 5/15 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 3 2-Propenal, 3-(3,4-dimethox... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T.

22.58 0.23 ug/L 208951 Phenant hranene - dl 0 22.95 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 42 2 Thiocyanic acid, 2-benzothiazoly... 192 C8H4N2S2 006011-99-0/40 3 1,2-Phenylene diisothiocyanate 192 C8H4N2S2 071105-17-4 38 4 Anthracene, 9-methyl- 192 C15H12 000779-02-2 38 Abundance Scan 3318 (22.574 min): 11416. D (-3311) (-) m/z 192.10 100.00% 192

5000

O-T 44 66 82 TTHTTTTTTTTTTTTTTTTTTHTTTTTTTHTTTTTTPTTWWPPTPTTTT Hr 118 146 160 | 22.20 22.40 22.60 22.80 23.00 m/z 191.00 17.74%| i'" 11"' ■ i m/z-> 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #80953: 2-Propenal, 3-(3,4-dimethoxyphenyl)- 192 161

5000 22.20 22.40 22.60 22.80 23.00 77 121 149 177 m/z 146.10 12.65% 91 103 52ill 64ii l 1I 138 O-T i'I ""i l m 11'1 - > pin ।. 11 I 1‘1T 1.1|..... Il ‘ "1111" 1 ’I I" "I TpT m/z-> 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #80870: Thiocyanic acid, 2-benzothiazolyl ester 192 . ............ ,. ।, p 22.20 22.40 22.60 22.80 23.00 5000 m/z 96.00 12.32%|

45 6990 108 122 134| 148 160 O-T mPP HHHHHH+L, T TTHTTmpTT ITT /z-> 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #80862:1,2-Phenylene diisothiocyanate 1 1 1 1 ' 1 1 1 1 1 1 1 ‘ I ' ■ TI" 192 22.20 22.40 22.60 22.80 23.00 m/z 193.10 11.93%| 64 5000

39 50 75 90 134 A

m/z-> 0 nMf.. 18.2817 1—+++++++#+*+ J 107 122, " "I‘l I I'l I I I I I'l I I I P I'l I I 148 160 "1 r'111" " r1" i" " i IT 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 22.20 22.40 22.60 22.80 23.00

11416.D 050102.M Tue May 21 15:58:25 2002 Page 5 .

NYC-WTC_000025341

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NYC-WTC_000025341Source: NYC Law Department, mirrored locally

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GC/MS analysis results for sample AE11412, May 28 2002 · Box DEP Box 18

NYC-WTC_000025257

Laboratory report showing gas chromatography/mass spectrometry results for sample AE11412 analyzed on May 28, 2002.

1 shared topics · Same agency, volume and box · similarity 0.995