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GCMS analysis results for sample AE11409, May 22 2002

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Laboratory report showing GCMS analysis results for sample AE11409 conducted on May 22, 2002.

NYC-WTC_000025182–000025195

Folder label: “GCMS X 5/15/02 A 5/17/02

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Data File : C:\MSDCHEM\1\DATA\051702\11384.D Vial : 11 Acq On : 17 May 2002 8:56 pm Operator: Mclean Sample : 5/15 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHCDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 5 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.43 ug/L 436108 Phenanthranene-dl0 22.95 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-diO- 188 C14D10 001719-06-8 72 2 Pentacyclo[7.3.1.1.(4,12).0(2,7)... 188 C14H20 1000215-61-8 64. 3 Pentacyclo[8.4.0.0(3,7).0(4,14).... 188 C14H20 1000099-27-2 38 U 4 Phenanthrene-diO 188 C14D10 001517-22-2 33 - Abundance Scan 3409 (23.109 min): 11384.D (-3401) (-) m/z 188.10 100.00% its

5000 ._________________ 80 94 160 22.80 23.00 23.20 23.40

m/z—> OT 111 40 -HHL L 66 H I 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ITT m/Z 189.10 ft 16.42% Abundance #79826: Anthracene-d ID- 1tS

5000 22.80 23.00 23.20 23.40 m/ z 80.10 15.20% 80 94 160 17 30 42 52 , 66 1J 108 118 132 146 11170179 0-TPTTTTTTTTT T] t-1 I I ]'| 1 I I | n )'] I I l t ] t ! ! | | I ! J t |H n [ I I I J | I I I I | ! ! I""i I I | | 1 1 I | | 1’111 m/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79715: Pentacyclo[7.3.1 .1 .(4,12).0(2,7).0(6,11 )]tetradeca... US

22.80 23.00 23.20 23.40 5000 79 91 m/z 94.05 13.88% 55 67 105 117 131

m/z-> 0 ‘ i ■" ■ i" " i" " i" ml—ll L —llm 1451424373. 1 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79714: Pentacyclo[8.4.0.0(3,7).0(4,14).0(6,11 )]tetradecane 1 ' I ' 1 ' 1 1 ' r ' ■ I ' ' ' ■ I us 22.80 23.00 23.20 23.40 m/z 160.10 9.01%

5000 79 91 . 117 131 145 159 173 . 106

/z-> 0 ,-i. n 27—55, L, . 1 L . TTH „ । AlI, । i'i trrrr 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ..... I..... 22.80 23.00 23.20 23.40

11384.D 050102.M Tue May 21 11:56:21 2002 Page 8

NYC-WTC_000025194

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NYC-WTC_000025194Source: NYC Law Department, mirrored locally

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