GCMS analysis results for sample AE11409, May 22 2002

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Laboratory report showing GCMS analysis results for sample AE11409 conducted on May 22, 2002.

NYC-WTC_000025182–000025195

Folder label: “GCMS X 5/15/02 A 5/17/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\051702\11384 .D Vial: 11 Acq On : 17 May 2002 8:56 pm Operator: Mclean Sample : 5/15 ad Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 4 4-Hydroxy-3,5-dimethyleinna... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

22.58 0.26 ug/L 261904 Phenanthranene-dl0 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual

l 4-Hydroxy-3,5-dimethylcinnamic acid 192 C11H1203 1000132-15-8 59 a A 2 Anthracene, 2-methyl- 192 C15H12 000613-12-7 59/V 3 3-(2-Methoxy-5-methylphenyl)acry... 192 C11H1203 103986-76-1 40 J 4 Isoquinoline, 1,2,3,4-tetrahydro... 328 C18H20N2O4 1000128-79-2 40 Abundance Scan 3319 (22.580 min): 11384. D (-3309) (-) “m/z 192.0 0 100.00% 192

5000 .............. .. ..................... _ 82 96 146 160 22.20 22.40 22.60 22.80 23.00 66 । । 118 | # oV T--*HpH m/z 191.10 22.86% m/z-> 20 30 40 50 60 70 80 90.100 110 120 130 140 150 160 170 180 190 200 Abundance #81030: 4-Hydroxy-3,5-dimethylcinnamic acid 192

5000 ,.... A 22.20 22.40 22.60 22.80 23.00 89 175 m/z 193.00 14.86% 63 145 117 45 53 77 j 0 --HHH— 105 TTpnmtTT TTr 135 | 163 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 .140 150 160 170 180 190 200 Abundance #125847: Anthracene, 2-methyl- 192 TT T 1 22.20 22.40 22.60 22.80 23.00 5000 m/z 146.10 13.52%

28 39 51 63 74 82 96 115 126 139 152 165 176 | 0-TITTTTUTTTTTTTTTTTTTTTTTTNTTLTTTITTTTTTTTTTTTTTTTTTTTTHTT m/z-> :20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80954: 3-(2-Methoxy-5-methylphenyl)acrylic acid ■ i ■ ' ■ ■ r1 1 i ■ ■ ■ 1 i 1 161 192 22.20 22.40 22.60 22.80 23.00 m/ Z 96.00 11.36%

5000 105 77 132 91 115 . 145 A n/z-> 0 39 51 65 111' " I' " lt r lurrkr l p+llpiyilu—... l hi , 175 - 4uug 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 ■ i ' ' 1 ' i ‘ ■ 1 i ' ' 1 1 i ' ' 22.20 22.40 22.60 22.80 23.00 "di"

11384.D 050102.M Tue May 21 11:56:18 2002 Page 7

NYC-WTC_000025193

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