GCMS blank analysis results for sample AE09329, May 7 2002

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Data File C:\MSDCHEM\1\DATA\050202\0429LB.D Vial: 6 Acq On 2 May 2002 3:38 pm V Operator: Mclean Sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 4 Phenanthrene-dlO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 23.11 0.65 ug/L 446810 Phenanthranene-dl0 22.95 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-dlO 188 C14D10 001517-22-2 94 2 Anthracene-dlO- 188 C14D10 001719-06-8 90 3 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 42 4 3H-Pyrazol-3-one, 2,4-dihydro-4,... 188 C11H12N2O 017694-06-3 40 Abundance Scan 3409 (23.109 min): 0429LB.D (-3402) (-) m/z 188.10 100.00% 188

5000 r ' i ' 1 ' — >—> ■ । ■ ' . > । । । । । । 80 94 160 22.80 23.00 23.20 23.40 40 54 66 11 132 hl I, I 111'11 i | । i । i । i I i । । i । I । । i i < I j i i । i । । Li J ri i i । i i i i । i i i i [ / । । । । rri i । i । II | i i 11 । rrn 1 r-- i11" i m/ z 94.10 15.88% /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188

5000 22.80 23.00 23.20 23.40 m/z 160.10 13.71% 80 94 160 30 42 52 66 11 | r i i r | i i Pi | I notovvpl I i i । I I I i | . il 108 118 132 146 1 . .................... TT I 1 I I | I I I I | I I I I | I ’ I I | I I I I | I I I I | I I I T | I I' I 'I | > I i i | I I ■ I | I | | I | i I I | |

/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d 10- 188

22.80 23.00 23.20 23.40 5000 m/z 189.10 13 .37%

80 94 160 , . 17 30 42 52 66 + 108 118 132 146 ,|.| 1701791.1 | 1111 ri j"11 ri । ■ 111"! 111111111111111 । | I । 1 I । । । । i । t I । i | I I I । । i r I r । i I I'!1 |*r i i i । i i i i | I '14 I | । i । i । m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79771:3-Amino-4-methyl-6-methoxyquinoline ........................ ............................. 1 ■ i 1 1 ' ' r 1 1 1 ■ । 1 1 1 1 । .' 1 1 1 i 188 22.80 23.00 23.20 23.40 m/z80.05 12.56%l 145 5000

117 41 51 63 77 89 102 1 30 i |-| ■ | i j i ■ I i । i i i i AI- mlert rlln । i Plh'l i l rlll-l , r l- rp r|l. i i i I i i I 159 173 Ihl..... -P i । । । P । । > — i [ । । । । । ।—।—।—।—[■ TTIIll /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

0429LB.D 050102.M Mon May 06 10:58:31 2002 Page 7

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